Kulczyk Mariusz, Skiba Jacek, Skorupska Monika, Przybysz Sylwia, Smalc-Koziorowska Julita
Institute of High Pressure Physics, Polish Academy of Sciences (Unipress), Sokołowska 29/37, 01-142 Warsaw, Poland.
Materials (Basel). 2022 Jul 14;15(14):4892. doi: 10.3390/ma15144892.
The study presents an analysis of the influence of the plastic strain rate on the mechanical and structural properties of pure zinc. Thanks to the use of unconventional methods of plastic processing, the process of the equal channel angular pressing (ECAP) and the process of hydrostatic extrusion (HE), the tests were performed in a wide range of plastic strain rates, between 0.04 s and 170 s. Plastic strain rate changes were carried out in the course of the significant plastic strain processes, and not on previously deformed samples. All tests were carried out at a constant value of plastic strain rate, ε ~ 2. A strong influence of the plastic strain rate on changes in the microstructure in zinc was observed during the tests. For the rates in the range of 0.04 s to 0.53 s its bimodal nature was observed, and in the range of 7 s to 170 s high homogeneity and evenness of grains related to the processes of continuous dynamic recrystallization was noticed. The effect of the strong homogenization of the microstructure was the increase in mechanical properties, yield point and tensile strength to the maximum values of UTS = 194 MPa, YS = 145 MPa at a strain rate of 170 s. Compared to the material with a bimodal microstructure, an over seven-fold increase in the elongation value was observed.
该研究分析了塑性应变速率对纯锌力学性能和结构性能的影响。由于采用了非常规的塑性加工方法,即等径角挤压(ECAP)工艺和静液挤压(HE)工艺,测试在0.04 s至170 s的宽塑性应变速率范围内进行。塑性应变速率的变化是在显著塑性应变过程中进行的,而不是在先前变形的样品上进行。所有测试均在塑性应变速率的恒定值ε~2下进行。测试过程中观察到塑性应变速率对锌微观结构变化有强烈影响。对于0.04 s至0.53 s范围内的应变速率,观察到其具有双峰性质,而在7 s至170 s范围内,注意到与连续动态再结晶过程相关的晶粒具有高均匀性和均匀度。微观结构强烈均匀化的效果是力学性能的提高,在应变速率为170 s时,屈服点和抗拉强度达到UTS = 194 MPa、YS = 145 MPa的最大值。与具有双峰微观结构的材料相比,伸长率值增加了七倍以上。