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AlSi7Mg0.6铝合金粉末再利用对激光粉末床熔融成型(LPBF)样品质量和力学性能的影响

Influence of the AlSi7Mg0.6 Aluminium Alloy Powder Reuse on the Quality and Mechanical Properties of LPBF Samples.

作者信息

Smolina Irina, Gruber Konrad, Pawlak Andrzej, Ziółkowski Grzegorz, Grochowska Emilia, Schob Daniela, Kobiela Karol, Roszak Robert, Ziegenhorn Matthias, Kurzynowski Tomasz

机构信息

Centre for Advanced Manufacturing Technologies (CAMT-FPC), Faculty of Mechanical Engineering, Wroclaw University of Science and Technology, ul. Łukasiewicza 5, 50-371 Wroclaw, Poland.

Chair of Engineering Mechanics and Machine Dynamics, Brandenburg University of Technology Cottbus-Senftenberg, Universitätsplatz 1, 01968 Senftenberg, Germany.

出版信息

Materials (Basel). 2022 Jul 19;15(14):5019. doi: 10.3390/ma15145019.

Abstract

Additive manufacturing (AM) is dynamically developing and finding applications in different industries. The quality of input material is a part of the process and of the final product quality. That is why understanding the influence of powder reuse on the properties of bulk specimens is crucial for ensuring the repeatable AM process chain. The presented study investigated the possibility of continuous reuse of AlSi7Mg0.6 powder in the laser powder bed fusion process (LPBF). To date, there is no study of AlSi7Mg0.6 powder reuse in the LPBF process to be found in the literature. This study aims to respond to this gap. The five batches of AlSi7Mg0.6 powder and five bulk LPBF samples series were characterised using different techniques. The following characteristics of powders were analysed: the powder size distribution (PSD), the morphology (scanning electron microscopy-SEM), the flowability (rotating drum analysis), and laser light absorption (spectrophotometry). Bulk samples were characterised for microstructure (SEM), chemical composition (X-ray fluorescence spectrometry-XRF), porosity (computed tomography-CT) and mechanical properties (tensile, hardness). The powder was reused in subsequent processes without adding (recycling/rejuvenation) virgin powder (collective ageing powder reuse strategy). All tested powders (powders P0-P4) and bulk samples (series S0-S3) show repeatable properties, with changes observed within error limits. Samples manufactured within the fifth reuse cycle (series S4) showed some mean value changes of measured characteristics indicating initial degradation. However, these changes also mostly fit within error limits. Therefore, the collective ageing powder reuse strategy is considered to give repeatable LPBF process results and is recommended for the AlSi7Mg0.6 alloy within at least five consecutive LPBF processes.

摘要

增材制造(AM)正在蓬勃发展,并在不同行业中得到应用。原材料的质量是工艺过程和最终产品质量的一部分。因此,了解粉末再利用对块状试样性能的影响对于确保增材制造工艺链的可重复性至关重要。本研究探讨了在激光粉末床熔融工艺(LPBF)中连续再利用AlSi7Mg0.6粉末的可能性。迄今为止,尚未在文献中找到关于LPBF工艺中AlSi7Mg0.6粉末再利用的研究。本研究旨在填补这一空白。使用不同技术对五批AlSi7Mg0.6粉末和五个块状LPBF样品系列进行了表征。分析了粉末的以下特性:粉末粒度分布(PSD)、形态(扫描电子显微镜-SEM)、流动性(转鼓分析)和激光吸收率(分光光度法)。对块状样品的微观结构(SEM)、化学成分(X射线荧光光谱法-XRF)、孔隙率(计算机断层扫描-CT)和力学性能(拉伸、硬度)进行了表征。粉末在后续工艺中进行再利用,不添加(回收/再生)原始粉末(集体时效粉末再利用策略)。所有测试粉末(粉末P0-P4)和块状样品(系列S0-S3)均显示出可重复的性能,观察到的变化在误差范围内。在第五次再利用循环中制造的样品(系列S4)显示出一些测量特性的平均值变化,表明开始出现降解。然而,这些变化大多也在误差范围内。因此,集体时效粉末再利用策略被认为能够给出可重复的LPBF工艺结果,并且建议在至少连续五个LPBF工艺中用于AlSi7Mg0.6合金。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/8d8e/9318767/98ca6e72ce55/materials-15-05019-g001.jpg

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