Ouyang Qijian, Xie Zhiwei, Liu Jinhai, Gong Minghui, Yu Huayang
School of Civil Engineering and Transportation, South China University of Technology, Guangzhou 510641, China.
State Key Laboratory of High Performance Civil Engineering Materials, Nanjing 210096, China.
Polymers (Basel). 2022 Jul 13;14(14):2851. doi: 10.3390/polym14142851.
In the past three decades, researchers have engaged in the relationship between the composition, macro performance, and microstructure of asphalt. There are many research results in the use of atomic force microscopy (AFM) to study the microstructure and related mechanisms of asphalt. Based on previous studies, the performance of asphalt from its microstructure has been observed and analyzed, and different evaluation indices and modification methods have been proposed, providing guidance toward improving the performance of asphalt materials and benefiting potential applications. This review focuses on the typical application and analysis of AFM in the study of the aging regeneration and modification properties of asphalt. Additionally, this review introduces the history of the rheological and chemical testing of asphalt materials and the history of using AFM to investigate asphalt. Furthermore, this review introduces the basic principles of various modes of application of AFM in the microstructure of asphalt, providing a research direction for the further popularization and application of AFM in asphalt or other materials in the future. This review aims to provide a reference and direction for researchers to further popularize the application of AFM in asphalt and standardize the testing methods of AFM. This paper is also helpful in further exploring the relationship between the microstructure and macro performance of asphalt.
在过去三十年中,研究人员一直致力于研究沥青的组成、宏观性能和微观结构之间的关系。在使用原子力显微镜(AFM)研究沥青的微观结构及相关机理方面有许多研究成果。基于以往的研究,已从沥青的微观结构观察和分析了其性能,并提出了不同的评价指标和改性方法,为改善沥青材料性能及潜在应用提供了指导。本综述重点关注AFM在沥青老化再生和改性性能研究中的典型应用与分析。此外,本综述介绍了沥青材料流变学和化学测试的历史以及使用AFM研究沥青的历史。再者,本综述介绍了AFM在沥青微观结构中各种应用模式的基本原理,为未来AFM在沥青或其他材料中的进一步推广应用提供了研究方向。本综述旨在为研究人员进一步推广AFM在沥青中的应用并规范AFM测试方法提供参考和方向。本文也有助于进一步探索沥青微观结构与宏观性能之间的关系。