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用于定量测定姜黄粉中姜黄素类化合物的台式和便携式近红外及拉曼光谱方法的比较研究

A Comparative Study of Benchtop and Portable NIR and Raman Spectroscopic Methods for the Quantitative Determination of Curcuminoids in Turmeric Powder.

作者信息

Khongkaew Putthiporn, Cruz Jordi, Bertotto Judit Puig, Cárdenas Vanessa, Alcalà Manel, Nuchtavorn Nantana, Phechkrajang Chutima

机构信息

Department of Pharmaceutical Chemistry, Faculty of Pharmacy, Mahidol University, Bangkok 10400, Thailand.

Faculty of Pharmaceutical Science, Burapha University, Chonburi 20131, Thailand.

出版信息

Foods. 2022 Jul 22;11(15):2187. doi: 10.3390/foods11152187.

Abstract

Turmeric consumption is continually increasing worldwide. Curcuminoids are major active constituents in turmeric and are associated with numerous health benefits. A combination of spectroscopic methods and chemometrics shows the suitability of turmeric for food quality control due to advantages such as speed, versatility, portability, and no need for sample preparation. Five calibration models to quantify curcuminoids in turmeric were proposed using benchtop and portable devices. The most remarkable results showed that Raman and NIR calibration models present an excellent performance reporting RMSEP of 0.44% / and 0.41% /, respectively. In addition, the five proposed methods (FT-IR, Raman, and NIR) were compared in terms of precision and accuracy. The results showed that benchtop and portable methods were in good agreement and that there are no significant differences between them. This study aims to foster the use of portable devices for food quality control in situ by demonstrating their suitability for the purpose.

摘要

全球范围内姜黄的消费量持续增长。姜黄素类化合物是姜黄中的主要活性成分,具有众多健康益处。光谱方法与化学计量学相结合表明,姜黄因其速度快、通用性强、便携且无需样品制备等优点,适用于食品质量控制。使用台式和便携式设备提出了五种用于定量姜黄中姜黄素类化合物的校准模型。最显著的结果表明,拉曼和近红外校准模型表现出色,RMSEP分别为0.44%和0.41%。此外,对所提出的五种方法(傅里叶变换红外光谱法、拉曼光谱法和近红外光谱法)的精密度和准确性进行了比较。结果表明,台式和便携式方法具有良好的一致性,它们之间没有显著差异。本研究旨在通过证明便携式设备适用于该目的,促进其在食品质量现场控制中的应用。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/578d/9331271/1be8ead86234/foods-11-02187-g001.jpg

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