Wei Shasha, Wang Renxin, Yang Hu, Guo Ziming, Lin Rongchuan, Huang Qingmin, Zhou Yuhui
College of Marine Equipment and Mechanical Engineering, Jimei University, Xiamen 361021, China.
Materials (Basel). 2022 Jul 25;15(15):5153. doi: 10.3390/ma15155153.
An AlCrSiWN coating was prepared on a cemented carbide substrate by the arc ion plating technology. The optimization of the coating process was carried out by matrix analysis of orthogonal experiments to calculate the influence of the process parameters on the hardness, bonding and roughness indexes of the coating, determine the optimal coating process parameters, and focus on the influence of the bias voltage on the microscopic morphology, mechanical properties and friction properties of the coating. The results showed that the influence of the process parameters on the indexes of the orthogonal experiments was in the following order: bias voltage > arc current > N2 flow rate. The optimal solution was achieved with an arc current of 160 A, a bias voltage of −80 V, and a N2 flow rate of 600 sccm. Properly increasing the bias voltage improved the microscopic morphology, mechanical properties and wear resistance of the coating. When the bias voltage was −80 V, the coating surface presented fewer large particles with a less uniform size and no obvious crater defects; in addition, the cross-sectional structure changed from grape-like to columnar, and the coating had higher hardness, lower roughness and better bond strength. In the friction performance test, coating at a −80 V bias voltage showed better wear resistance, which was reflected in lower friction coefficient and wear, and the wear mechanism mainly consisted of adhesion and oxidation wear.
采用电弧离子镀技术在硬质合金基体上制备了AlCrSiWN涂层。通过正交试验的矩阵分析对涂层工艺进行优化,以计算工艺参数对涂层硬度、结合力和粗糙度指标的影响,确定最佳涂层工艺参数,并重点研究偏压对涂层微观形貌、力学性能和摩擦性能的影响。结果表明,工艺参数对正交试验指标的影响顺序为:偏压>电弧电流>N2流量。在电弧电流为160 A、偏压为−80 V、N2流量为600 sccm时获得了最优解。适当提高偏压可改善涂层的微观形貌、力学性能和耐磨性。当偏压为−80 V时,涂层表面大颗粒较少,尺寸均匀性较差,无明显坑洼缺陷;此外,横截面结构从葡萄状变为柱状,涂层具有较高的硬度、较低的粗糙度和较好的结合强度。在摩擦性能测试中,偏压为−80 V的涂层表现出较好的耐磨性,表现为较低的摩擦系数和磨损,磨损机制主要为粘着磨损和氧化磨损。