Al-Dulaijan Yousif A, Alsulaimi Leenah, Alotaibi Reema, Alboainain Areej, Akhtar Sultan, Khan Soban Q, Al-Ghamdi Maram, Gad Mohammed M
Department of Substitutive Dental Sciences, College of Dentistry, Imam Abdulrahman Bin Faisal University, Dammam, Saudi Arabia.
College of Dentistry, Imam Abdulrahman Bin Faisal University, Dammam, Saudi Arabia.
J Prosthodont. 2023 Apr;32(S1):45-52. doi: 10.1111/jopr.13572. Epub 2022 Aug 16.
To evaluate the effect of printing orientation combined with different postcuring times on the flexural strength of 3D-printed resins.
A total of 480 rectangular specimens with the dimensions of 64×10×3.3 mm were designed and fabricated from two 3D-printed acrylic resins and one heat-polymerized resin (HP). 3D-printed groups were divided into 3 groups according to printing orientations (0-, 45-, 90-degree); each group was subdivided into 4 groups according to postcuring time (30, 60, 90, 120 min.). All specimens were subjected to thermal cycling (10,000 cycles) before testing flexural strength. Fractured surfaces were examined under a scanning electron microscope (SEM). ANOVA and Tukey's post hoc tests were used for data analysis (α = 0.05).
The result of this study showed that the highest flexural strength values of 3D-printed resin (NextDent, and ASIGA) were in 0-degree groups. Also, the flexural strength values increased when postcuring time was increased, regardless of the printing orientation; the highest flexural strength was recorded at 120 minutes postcuring time in all orientations. SEM analysis showed a rougher surface with irregular lamellae which represented a ductile fracture confirming that high energy is required for crack propagation and these features markedly increased as postcuring time increased.
The results showed that the 0-degree orientation groups showed higher flexural strength compared to other groups. Similarly, with increased postcuring time, the flexural strength increased.
评估打印方向与不同后固化时间相结合对3D打印树脂弯曲强度的影响。
用两种3D打印丙烯酸树脂和一种热聚合树脂(HP)设计并制作了480个尺寸为64×10×3.3mm的矩形试件。3D打印组根据打印方向(0度、45度、90度)分为3组;每组根据后固化时间(30、60、90、120分钟)再细分为4组。所有试件在测试弯曲强度前均进行热循环(10000次循环)。在扫描电子显微镜(SEM)下检查断裂表面。采用方差分析和Tukey事后检验进行数据分析(α = 0.05)。
本研究结果表明,3D打印树脂(NextDent和ASIGA)的最高弯曲强度值出现在0度组。此外,无论打印方向如何,后固化时间增加时弯曲强度值都会增加;所有方向在后固化120分钟时记录到最高弯曲强度。SEM分析显示表面更粗糙,有不规则薄片,代表韧性断裂,证实裂纹扩展需要高能量,且随着后固化时间增加这些特征明显增加。
结果表明,0度方向组的弯曲强度高于其他组。同样地,随着后固化时间增加,弯曲强度增加