Matsui J, Takatsu K, Tsusaka Y
Synchrotron Radiation Research Center, Hyogo Science and Technology Association, 1-490-2 Kouto, Shingu, Tatsuno, Hyogo 679-5165, Japan.
Graduate School of Science, University of Hyogo, 3-2-1 Kouto, Kamigori, Hyogo 678-1297, Japan.
J Synchrotron Radiat. 2022 Sep 1;29(Pt 5):1251-1257. doi: 10.1107/S1600577522007779. Epub 2022 Aug 17.
X-ray topography exerting the super-Borrmann effect has been performed using synchrotron radiation to display dislocation images with a high-speed and high-resolution CMOS camera. Forward-transmitted X-rays are positively employed instead of reflected X-rays to reveal dislocations in relatively thick crystals by simultaneously exciting a pair of adjacent {111} planes owing to the super-Borrmann effect. Before the experiment, minimum values of the attenuation coefficients A for σ and π polarizations of the incident X-rays in the three-beam case are calculated. Results demonstrate that A for both polarizations are almost 20 times larger than those in the two-beam (usual Borrmann effect) case. The transmitted X-rays can be used to confirm the efficacy of taking topographs under the super-Borrmann conditions, as well as under multiple-diffraction conditions. Furthermore, super-Borrmann topographs can be considered for relatively thick crystals, where a conventional Lang X-ray topography technique is difficult to apply.
利用同步辐射进行了产生超博尔曼效应的X射线形貌术,并用高速高分辨率CMOS相机显示位错图像。通过超博尔曼效应同时激发一对相邻的{111}平面,正向透射的X射线被积极地用于代替反射X射线,以揭示相对较厚晶体中的位错。在实验之前,计算了三光束情况下入射X射线的σ和π偏振的衰减系数A的最小值。结果表明,两种偏振的A值几乎比双光束(通常的博尔曼效应)情况下大20倍。透射的X射线可用于确认在超博尔曼条件下以及多衍射条件下拍摄形貌图的效果。此外,对于相对较厚的晶体,可以考虑使用超博尔曼形貌术,而传统的朗氏X射线形貌技术难以应用于此类晶体。