Okitsu Kouhei, Imai Yasuhiko, Ueji Yoshinori, Yoda Yoshitaka
Engineering Research Institute, School of Engineering, The University of Tokyo, Yayoi, Bunkyo-ku, Tokyo 113-8656, Japan.
Acta Crystallogr A. 2003 Jul;59(Pt 4):311-6. doi: 10.1107/s0108767303009036. Epub 2003 Jun 26.
A 'six-beam X-ray section topograph' experiment was performed whose images are in excellent agreement with the images computer-simulated using the theory derived by one of the authors [Okitsu (2003). Acta Cryst. A59, 235-244] based on the Takagi-Taupin dynamical theory. X-rays whose wavefront was limited to 0.1 x 0.1 mm were incident on a [1 1; 1]-oriented floating-zone silicon crystal with thickness of 9.911 mm so that a six-beam condition was satisfied. The six reflection indices were 000 (forward diffraction), 440, 484, 088, 4;48 and 4;04. The plane of incidence of the 088 reflection was adjusted so as to be perpendicular to the direction of the incident horizontal linear polarization of the synchrotron radiation, which was monochromated into 18.5 keV (0.670 A wavelength). While the simulations were performed under the assumptions that the incident X-rays were linearly polarized both horizontally and vertically, they were evidently different and only the simulated images under the assumption of horizontally polarized incident X-rays were in excellent agreement with the images obtained by the experiment.
进行了一次“六束X射线截面形貌”实验,其实验图像与使用其中一位作者[Okitsu (2003). Acta Cryst. A59, 235 - 244]基于Takagi - Taupin动力学理论推导得出的理论进行计算机模拟得到的图像高度吻合。波前限制在0.1×0.1毫米的X射线入射到厚度为9.911毫米、取向为[1 1; 1]的浮区硅晶体上,从而满足六束条件。六个反射指数分别为000(正向衍射)、440、484、088、4;48和4;04。调整088反射的入射平面,使其垂直于同步辐射水平线性偏振的入射方向,同步辐射经单色化后波长为18.5 keV(0.670 Å)。虽然模拟是在入射X射线水平和垂直方向均为线性偏振的假设下进行的,但它们明显不同,只有在入射X射线水平偏振假设下的模拟图像与实验获得的图像高度吻合。