Chen Xingshuo, Jiang Shan, Li Yubo, Jiang Yanxiu, Wang Wei
Opt Express. 2022 Oct 24;30(22):40842-40853. doi: 10.1364/OE.469374.
The high-aspect-ratio silicon grating (HARSG) is an important X-ray optical device that is widely used in X-ray imaging and spectrum detection systems. In this paper, we propose a high-precision alignment method based on the scanning beam interference lithography (SBIL) system to realize precise alignment between the <111> orientation on the (110) wafer plane and the grating lines direction, which is an essential step in HARSG manufacture to obtain the high-aspect-ratio grating structure. After the location of the <111> orientation through fan-shaped mask etching and reference grating fabrication, a two-step method that combines static preliminary alignment and dynamic precision alignment is used to align the reference grating lines direction with the interference field fringes of the SBIL system through the interference of the diffracted light from the reference grating near the normal direction, which can realize a minimal alignment error of 0.001°. Through the overall alignment process, HARSGs with groove densities of 500 gr/mm, 1800 gr/mm, and 3600 gr/mm were fabricated through anisotropic wet etching in KOH solution, producing ultra-high aspect ratios and etch rate ratios greater than 200.
高深宽比硅光栅(HARSG)是一种重要的X射线光学器件,广泛应用于X射线成像和光谱检测系统。本文提出了一种基于扫描光束干涉光刻(SBIL)系统的高精度对准方法,以实现(110)晶圆平面上的<111>取向与光栅线方向之间的精确对准,这是HARSG制造中获得高深宽比光栅结构的关键步骤。通过扇形掩模蚀刻和参考光栅制作确定<111>取向位置后,采用静态初步对准和动态精密对准相结合的两步法,通过参考光栅在法线方向附近的衍射光干涉,使参考光栅线方向与SBIL系统的干涉场条纹对准,可实现最小0.001°的对准误差。通过整个对准过程,在KOH溶液中通过各向异性湿法蚀刻制造出了槽密度为500 gr/mm、1800 gr/mm和3600 gr/mm的HARSG,产生了超高深宽比和大于200的蚀刻速率比。