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Pyrazine-2(1)-thione.

作者信息

Olszewski Adrian, Wzgarda-Raj Kinga

机构信息

Department of Physical Chemistry, Faculty of Chemistry, University of Lodz, Pomorska 163/165, 90-236 Lodz, Poland.

出版信息

IUCrdata. 2021 Oct 29;6(Pt 10):x211102. doi: 10.1107/S2414314621011020. eCollection 2021 Oct.

DOI:10.1107/S2414314621011020
PMID:36340983
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC9462301/
Abstract

The title compound, CHNS, was obtained by the reduction of 2-mercapto-pyrazine (during its crystallization with 2-mercapto-pyrazine and isonicotinic acid -oxide in ethanol solution. It crystallizes in the monoclinic space group P. In the crystal, the mol-ecules are linked by N-H⋯N and C-H⋯S hydrogen bonds.

摘要
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/d19f/9462301/f6f5bad39c81/x-06-x211102-fig4.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/d19f/9462301/176e9b03a483/x-06-x211102-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/d19f/9462301/26a02019e0f6/x-06-x211102-fig2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/d19f/9462301/049f33dbcb63/x-06-x211102-fig3.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/d19f/9462301/f6f5bad39c81/x-06-x211102-fig4.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/d19f/9462301/176e9b03a483/x-06-x211102-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/d19f/9462301/26a02019e0f6/x-06-x211102-fig2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/d19f/9462301/049f33dbcb63/x-06-x211102-fig3.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/d19f/9462301/f6f5bad39c81/x-06-x211102-fig4.jpg

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本文引用的文献

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Substituted N-phenylpyrazine-2-carboxamides, their synthesis and evaluation as herbicides and abiotic elicitors.取代的N-苯基吡嗪-2-甲酰胺及其作为除草剂和非生物诱导剂的合成与评价
Molecules. 2007 Dec 20;12(12):2589-98. doi: 10.3390/12122589.
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A short history of SHELX.SHELX简史。
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Synthesis and preliminary evaluation of some pyrazine containing thiazolines and thiazolidinones as antimicrobial agents.一些含吡嗪的噻唑啉和噻唑烷酮类抗菌剂的合成及初步评价
Bioorg Med Chem. 2004 May 1;12(9):2151-61. doi: 10.1016/j.bmc.2004.02.024.
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Heterocyclic structures useful in medicinal chemistry: the case of pyrazino[2,3-c][1,2,6]thiadiazine 2,2-dioxide.
Farmaco. 1997 May;52(5):283-7.