Zhou Yongxin, Gu Yuandong, Zhang Songsong
School of Microelectronics, Shanghai University, Shanghai 200444, China.
Shanghai Industrial μTechnology Research Institute, Shanghai 201899, China.
Micromachines (Basel). 2022 Nov 5;13(11):1916. doi: 10.3390/mi13111916.
This paper introduces a novel nondestructive wafer scale thin film thickness measurement method by detecting the reflected picosecond ultrasonic wave transmitting between different interfacial layers. Unlike other traditional approaches used for thickness inspection, this method is highly efficient in wafer scale, and even works for opaque material. As a demonstration, we took scandium doped aluminum nitride (AlScN) thin film and related piezoelectric stacking layers (e.g. Molybedenum/AlScN/Molybdenum) as the case study to explain the advantages of this approach. In our experiments, a laser with a wavelength of 515 nm was used to first measure the thickness of (1) a single Molybdenum (Mo) electrode layer in the range of 100-300 nm, and (2) a single AlScN piezoelectric layer in the range of 600-1000 nm. Then, (3) the combined stacking layers were measured. Finally, (4) the thickness of a standard piezoelectric composite structure (Mo/AlScN/Mo) was characterized based on the conclusions and derivation extracted from the aforementioned sets of experiments. This type of standard piezoelectric composite has been widely adopted in a variety of Micro-electromechanical systems (MEMS) devices such as the Piezoelectric Micromachined Ultrasonic Transducer (PMUT), the Film Bulk Acoustic Resonator (FBAR), the Surface Acoustic Wave (SAW) and more. A comparison between measurement data from both in-line and off-line (using Scanning Electron Microscope) methods was conducted. The result from such in situ 8-inch wafer scale measurements was in a good agreement with the SEM data.
本文介绍了一种新颖的晶圆级薄膜厚度无损测量方法,该方法通过检测在不同界面层之间传输的反射皮秒超声波来实现。与用于厚度检测的其他传统方法不同,这种方法在晶圆级具有很高的效率,甚至适用于不透明材料。作为演示,我们以钪掺杂氮化铝(AlScN)薄膜和相关的压电堆叠层(例如钼/AlScN/钼)为例,解释了这种方法的优点。在我们的实验中,使用波长为515nm的激光首先测量了(1)厚度在100-300nm范围内的单个钼(Mo)电极层,以及(2)厚度在600-1000nm范围内的单个AlScN压电层。然后,(3)测量了组合的堆叠层。最后,(4)基于从上述几组实验中得出的结论和推导,对标准压电复合结构(Mo/AlScN/Mo)的厚度进行了表征。这种类型的标准压电复合材料已广泛应用于各种微机电系统(MEMS)器件中,如压电微机械超声换能器(PMUT)、薄膜体声波谐振器(FBAR)、表面声波(SAW)等。对在线和离线(使用扫描电子显微镜)方法的测量数据进行了比较。这种原位8英寸晶圆级测量的结果与扫描电子显微镜数据吻合良好。