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Determination of cyanide in blood by GC-MS using a new high selectivity derivatization reagent 1,2,3,3-tetramethyl-3H-indolium iodide.

作者信息

Morikawa Yasuhiro, Nishiwaki Keiji, Suzuki Shigeo, Shiomi Kazutaka, Nakanishi Isao

机构信息

Forensic Science Laboratory, Kyoto Prefectural Police H.Q., 85-3, Yabunouchi-cho, Kamigyo-ku, Kyoto, 602-8550, Japan.

Department of Pharmaceutical Sciences, Faculty of Pharmacy, Kindai University, 3-4-1, Kowakae, Higashiosaka, Osaka, 577-8502, Japan.

出版信息

Forensic Toxicol. 2022 Jul;40(2):393-399. doi: 10.1007/s11419-021-00610-w. Epub 2022 Jan 9.

DOI:10.1007/s11419-021-00610-w
PMID:36454401
Abstract
摘要

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Determination of cyanide in blood by GC-MS using a new high selectivity derivatization reagent 1,2,3,3-tetramethyl-3H-indolium iodide.使用新型高选择性衍生化试剂1,2,3,3-四甲基-3H-碘化吲哚鎓通过气相色谱-质谱联用仪测定血液中的氰化物
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引用本文的文献

1
Spectral and theoretical analysis of derivatives of 1,2,3,3-tetramethyl-3H-indolium iodide (TMI), a highly selective derivatization reagent of cyanide, and their utility for the analysis of cyanide concentrations in beverages.1,2,3,3-四甲基-3H-吲哚𬭩碘化物(TMI)衍生物的光谱和理论分析,TMI 是一种对氰化物具有高选择性的衍生化试剂,及其在饮料中氰化物浓度分析中的应用。
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本文引用的文献

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Gas chromatography-mass spectrometric identification of cyanide using a nucleophilic substitution based derivatization with -phenyl benzenethiosulfonate.使用基于亲核取代反应的衍生化试剂 - 苯并噻吩硫代磺酸钠对氰化物进行气相色谱-质谱联用鉴定。
Anal Methods. 2020 Dec 23;12(48):5839-5845. doi: 10.1039/d0ay01643h.
2
A Screening Method for Cyanide in Blood by Dimethoxytriazinyl Derivatization-GC/MS.二甲基三嗪基衍生化-GC/MS 法测定血液中的氰化物。
J Chromatogr Sci. 2021 Jan 1;59(1):1-6. doi: 10.1093/chromsci/bmaa081.
3
Rationally designed imidazole derivative as colorimetric and fluorometric sensor for selective, qualitative and quantitative cyanide ion detection in real time samples.
理性设计的咪唑衍生物作为比色和荧光传感器,用于实时样品中氰化物离子的选择性、定性和定量检测。
Spectrochim Acta A Mol Biomol Spectrosc. 2020 Jun 15;234:118212. doi: 10.1016/j.saa.2020.118212. Epub 2020 Mar 12.
4
Spontaneous optical response towards cyanide ion in water by a reactive binding site probe.通过反应结合位点探针对水中氰化物离子的自发光学响应。
Spectrochim Acta A Mol Biomol Spectrosc. 2020 Jun 5;233:118190. doi: 10.1016/j.saa.2020.118190. Epub 2020 Feb 24.
5
A coumarin-connected carboxylic indolinium sensor for cyanide detection in absolute aqueous medium and its application in biological cell imaging.一种香豆素连接羧酸吲哚𬭩传感器,用于在绝对水介质中检测氰化物及其在生物细胞成像中的应用。
Spectrochim Acta A Mol Biomol Spectrosc. 2020 Mar 5;228:117710. doi: 10.1016/j.saa.2019.117710. Epub 2019 Nov 1.
6
A review of rapid and field-portable analytical techniques for the diagnosis of cyanide exposure.用于诊断氰化物暴露的快速和现场便携式分析技术综述。
Anal Chim Acta. 2017 Apr 1;960:18-39. doi: 10.1016/j.aca.2016.12.039. Epub 2017 Jan 4.
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Inhal Toxicol. 2012 Feb;24(3):194-9. doi: 10.3109/08958378.2012.660285.
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J Anal Toxicol. 2011 Apr;35(3):143-7. doi: 10.1093/anatox/35.3.143.
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Clin Chem. 2006 Mar;52(3):458-67. doi: 10.1373/clinchem.2005.061002. Epub 2006 Jan 26.