Institute of Forensic Science, Public Security Bureau of Jiangyin, Jiangyin, 214431, China.
Institute of Forensic Science, Public Security Bureau of Wuxi, Wuxi, 214401, China.
Forensic Toxicol. 2022 Jan;40(1):163-172. doi: 10.1007/s11419-021-00605-7. Epub 2021 Dec 2.
The purpose of the current study was to evaluate an analytical characterization of a novel synthetic cannabinoid ethyl-2-(1-(5-fluoropentyl)-1H-indole-3-carboxamido)-3,3-dimethylbutanoate (5F-EDMB-PICA), which has a similar chemical structure to the controlled synthetic cannabinoid 5F-MDMB-PICA.
The compound was analyzed by gas chromatography-mass spectrometry (GC-MS), supercritical fluid chromatography-quadrupole time-of-flight-mass spectrometry (SFC-QTOF-MS) and spectroscopic methods, such as attenuated total reflection (ATR)-Fourier transform infrared (FTIR), ultraviolet-visible (UV-VIS) and nuclear magnetic resonance (NMR) spectroscopies.
In this study, we reported a comprehensive analytical data of 5F-EDMB-PICA. The data of analytical characterization for the 5F-EDMB-PICA were obtained by GC-MS, SFC-QTOF-MS, ATR-FTIR spectroscopy, UV-VIS spectroscopy, and H and C NMR spectroscopy.
In this study, we presented a comprehensive analytical characterization of 5F-EDMB-PICA obtained by H NMR, C NMR, GC-MS, SFC-QTOF-MS, ATR-FTIR spectroscopy and UV-VIS spectroscopy. The analytical data of 5F-EDMB-PICA are very useful for forensic, toxicological, and clinical diagnosis.
本研究的目的是评估一种新型合成大麻素乙基-2-（1-（5-氟戊基）-1H-吲哚-3-甲酰胺基）-3,3-二甲基丁酸酯（5F-EDMB-PICA）的分析特性，该化合物的化学结构与受管制的合成大麻素 5F-MDMB-PICA 相似。
该化合物通过气相色谱-质谱联用（GC-MS）、超临界流体色谱-四极杆飞行时间质谱（SFC-QTOF-MS）和衰减全反射（ATR）-傅里叶变换红外（FTIR）光谱、紫外-可见（UV-VIS）和核磁共振（NMR）光谱等光谱方法进行分析。
在本研究中，我们报道了 5F-EDMB-PICA 的综合分析数据。通过 GC-MS、SFC-QTOF-MS、ATR-FTIR 光谱、UV-VIS 光谱和 H 和 C NMR 光谱获得了 5F-EDMB-PICA 的分析特性数据。
在本研究中，我们通过 1H NMR、13C NMR、GC-MS、SFC-QTOF-MS、ATR-FTIR 光谱和 UV-VIS 光谱对 5F-EDMB-PICA 进行了全面的分析特性描述。5F-EDMB-PICA 的分析数据对于法医、毒理学和临床诊断非常有用。
