Gunderov Dmitriy, Asfandiyarov Rashid, Titov Vyacheslav, Gunderova Sofia, Astanin Vasily
Institute of Molecule and Crystal Physics of Ufa Federal Research Centre RAS, 151 Prospekt Oktyabrya Ave., 450075 Ufa, Russia.
Department of Materials Science and Physics of Metals, Ufa University of Science and Technology, 32 Zaki Validi Str., 450076 Ufa, Russia.
Materials (Basel). 2022 Dec 24;16(1):162. doi: 10.3390/ma16010162.
The effect of slippage during High Pressure Torsion (HPT) of technically pure Ti and pure Cu samples was investigated. The "joint torsion of the disk halves" method was used to evaluate the effect of slippage. It was shown that slippage starts already at the early stages of HPT. With a further increase in the number of revolutions , the slippage effect increases, and no torsional deformation occurs after = 5. The slippage effect is explained by analyzing the surface friction forces between the sample and the anvil. However, studies via TEM and XRD have shown that the structure of Ti samples after HPT at the investigated conditions is grinded to a nanocrystalline state. A structure is formed in Ti similar to that observed after HPT by other authors. The dislocation density increases with increasing HPT degree from = 5 to = 10 revolutions, despite slippage. Consequently, despite slippage at HPT at ≥ 5, deformation still occurs. The following assumptions are made to explain the accumulated strain in the sample at HPT. It is assumed that the planes of the upper and lower anvil during HPT are at a slight inclination relative to each other. Computer modeling using the Deform 3D software package has shown that this leads to the accumulations of significant strain during HPT.
研究了工业纯钛和纯铜样品在高压扭转(HPT)过程中的打滑效应。采用“盘片两半联合扭转”方法评估打滑效应。结果表明,打滑在HPT早期就已开始。随着扭转圈数的进一步增加,打滑效应增强,在扭转5圈后不再发生扭转变形。通过分析样品与砧座之间的表面摩擦力来解释打滑效应。然而,通过透射电子显微镜(TEM)和X射线衍射(XRD)研究表明,在所研究条件下,钛样品在HPT后的结构被研磨成纳米晶态。钛中形成的结构与其他作者在HPT后观察到的结构相似。尽管存在打滑现象,但随着HPT程度从5圈增加到10圈,位错密度仍会增加。因此,尽管在HPT扭转5圈及以上时存在打滑现象,但仍会发生变形。为了解释HPT过程中样品中的累积应变,做出了以下假设。假设HPT过程中上下砧座平面彼此略有倾斜。使用Deform 3D软件包进行的计算机模拟表明,这会导致HPT过程中产生显著的应变累积。