Ulrich L
Arch Toxicol. 1978 Dec 11;41(2):133-48. doi: 10.1007/BF00302525.
The dithizone extraction method has been applied in the determination of lead content in human bones. The lead in 21 samples of fresh vertebrae and ribs from autopsies is compared with the lead content of historical bones of 17 skeletons from 600--800 A.D. The preparation and the direct mineralization of the bones are presented. The lead content detected in the ash of bones is to low compared with the value found by direct wet mineralization of the bones. During the dry ashing process with temperatures of 500 degrees C or higher lead may be lost. For the same person the lead content of rib is always lower than the value found in vertebra. The difference of the lead content of fresh bones and the historical bones is only small. In both groups the lead content in the bones increased with age. Compared with studies of other authors in the time of 1930--1970 the results would suggest that the present intake of lead in accidental selected bones among a population situated in an appointed area is not greater than in the past.
双硫腙萃取法已应用于人体骨骼中铅含量的测定。将21份来自尸检的新鲜椎骨和肋骨样本中的铅含量与公元600 - 800年17具骨骼的历史骨骼中的铅含量进行了比较。介绍了骨骼的制备和直接矿化方法。与通过骨骼直接湿法矿化得到的值相比,在骨骼灰分中检测到的铅含量较低。在500摄氏度或更高温度的干灰化过程中,铅可能会损失。对于同一个人,肋骨中的铅含量总是低于椎骨中的值。新鲜骨骼和历史骨骼的铅含量差异很小。在两组中,骨骼中的铅含量都随着年龄的增长而增加。与1930 - 1970年其他作者的研究相比,结果表明,在指定区域的人群中,偶然选取的骨骼中目前的铅摄入量并不比过去大。