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涂覆有各种类型纳米颗粒的316L不锈钢的表面表征

Surface Characterization of Stainless Steel 316L Coated with Various Nanoparticle Types.

作者信息

Aldabagh Dhiaa J, Alzubaydi Thair L, Alhuwaizi Akram F

机构信息

Department of Orthodontics, College of Dentistry, University of Baghdad, Baghdad 00964, Iraq.

Department of Prosthodontic Dental Technology, Al-Esraa University College, Baghdad 00964, Iraq.

出版信息

Int J Biomater. 2023 Jan 25;2023:3997281. doi: 10.1155/2023/3997281. eCollection 2023.

DOI:10.1155/2023/3997281
PMID:36744019
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC9891840/
Abstract

BACKGROUND

Material tribology has widely expanded in scope and depth and is extended from the mechanical field to the biomedical field. The present study aimed to characterize the nanocoating of highly pure (99.9%) niobium (Nb), tantalum (Ta), and vanadium (V) deposited on 316L stainless steel (SS) substrates which considered the most widely used alloys in the manufacturing of SS orthodontic components. To date, the coating of SS orthodontic archwires with Nb, Ta, and V using a plasma sputtering method has never been reported. Nanodeposition was performed using a DC plasma sputtering system with three different sputtering times (1, 2, and 3 hours).

RESULTS

Structural and elemental analyses were conducted on the deposited coatings using XRD, FESEM, and EDS showing a unique phase of coating metals over their substrates with obvious homogeneous even deposition. A highly significant positive correlation was found between sputtering time and thickness of the achieved coatings. AFM revealed a reduction in the surface roughness of 316L SS substrates sputtered with all coating materials, significantly seen in V coatings.

CONCLUSIONS

Sputtering time and coating material play a significant role in terms of microstructure and topography of the achieved coatings being the best in the Ta group; moreover, surface roughness was significantly improved by V coatings. Likewise, it is found to be sputtering time independent for all used coatings.

摘要

背景

材料摩擦学在范围和深度上都有了广泛扩展，已从机械领域延伸到生物医学领域。本研究旨在表征沉积在316L不锈钢（SS）基体上的高纯度（99.9%）铌（Nb）、钽（Ta）和钒（V）的纳米涂层，316L不锈钢是制造正畸部件最常用的合金。迄今为止，尚未有使用等离子溅射法在正畸弓丝上涂覆Nb、Ta和V的报道。使用直流等离子溅射系统进行纳米沉积，溅射时间分别为1小时、2小时和3小时。

结果

使用X射线衍射（XRD）、场发射扫描电子显微镜（FESEM）和能谱仪（EDS）对沉积涂层进行结构和元素分析，结果表明涂层金属在其基体上呈现独特的相，且沉积均匀明显。溅射时间与所得涂层厚度之间存在极显著的正相关。原子力显微镜（AFM）显示，所有涂层材料溅射后的316L SS基体表面粗糙度均降低，其中V涂层降低尤为显著。

结论

溅射时间和涂层材料对所得涂层的微观结构和形貌有显著影响，Ta组效果最佳；此外，V涂层显著改善了表面粗糙度。同样，对于所有使用的涂层，表面粗糙度的改善与溅射时间无关。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/0ea4/9891840/b2a8b04b9a7d/IJBM2023-3997281.010.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/0ea4/9891840/a39ddb9b7a0c/IJBM2023-3997281.001.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/0ea4/9891840/85dca68dcfa0/IJBM2023-3997281.002.jpg
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https://cdn.ncbi.nlm.nih.gov/pmc/blobs/0ea4/9891840/dc59d48aa72b/IJBM2023-3997281.006.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/0ea4/9891840/034e5af07165/IJBM2023-3997281.007.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/0ea4/9891840/290b72212940/IJBM2023-3997281.008.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/0ea4/9891840/69027b39f76b/IJBM2023-3997281.009.jpg
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https://cdn.ncbi.nlm.nih.gov/pmc/blobs/0ea4/9891840/a39ddb9b7a0c/IJBM2023-3997281.001.jpg
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https://cdn.ncbi.nlm.nih.gov/pmc/blobs/0ea4/9891840/dc59d48aa72b/IJBM2023-3997281.006.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/0ea4/9891840/034e5af07165/IJBM2023-3997281.007.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/0ea4/9891840/290b72212940/IJBM2023-3997281.008.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/0ea4/9891840/69027b39f76b/IJBM2023-3997281.009.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/0ea4/9891840/b2a8b04b9a7d/IJBM2023-3997281.010.jpg

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