• 文献检索
  • 文档翻译
  • 深度研究
  • 学术资讯
  • Suppr Zotero 插件Zotero 插件
  • 邀请有礼
  • 套餐&价格
  • 历史记录
应用&插件
Suppr Zotero 插件Zotero 插件浏览器插件Mac 客户端Windows 客户端微信小程序
定价
高级版会员购买积分包购买API积分包
服务
文献检索文档翻译深度研究API 文档MCP 服务
关于我们
关于 Suppr公司介绍联系我们用户协议隐私条款
关注我们

Suppr 超能文献

核心技术专利：CN118964589B侵权必究
粤ICP备2023148730 号-1Suppr @ 2026

文献检索

告别复杂PubMed语法，用中文像聊天一样搜索，搜遍4000万医学文献。AI智能推荐，让科研检索更轻松。

立即免费搜索

文件翻译

保留排版，准确专业，支持PDF/Word/PPT等文件格式，支持 12+语言互译。

免费翻译文档

深度研究

AI帮你快速写综述，25分钟生成高质量综述，智能提取关键信息，辅助科研写作。

立即免费体验

TiSiC相的合成及MAX/SiC复合材料的固结——微观结构与力学性能

Synthesis of TiSiC Phases and Consolidation of MAX/SiC Composites-Microstructure and Mechanical Properties.

作者信息

Wozniak Jaroslaw, Petrus Mateusz, Cygan Tomasz, Adamczyk-Cieślak Boguslawa, Moszczyńska Dorota, Olszyna Andrzej Roman

机构信息

Faculty of Material Science and Engineering, Warsaw University of Technology, 02-507 Warsaw, Poland.

出版信息

Materials (Basel). 2023 Jan 17;16(3):889. doi: 10.3390/ma16030889.

DOI:10.3390/ma16030889
PMID:36769901
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC9917825/
Abstract

The article describes the TiSiC powder synthesis process. The influence of the molar ratio and two forms of carbon on the phase composition of the obtained powders was investigated. The synthesis was carried out using a spark plasma sintering (SPS) furnace. In addition, using the obtained powders, composites reinforced with SiC particles were produced. The obtained results showed no effect of the carbon form and a significant impact of annealing on the purity of the powders after synthesis. The composites were also consolidated using an SPS furnace at two temperatures of 1300 and 1400 °C. The tests showed low density and hardness for sinters from 1300 °C (maximum 3.97 g/cm and 447 HV5, respectively, for composite reinforced with 10% SiC). These parameters significantly increase for composites sintered at 1400 °C (maximum density 4.43 g/cm and hardness 1153 HV5, for TiAlC-10% SiC). In addition, the crack propagation analysis showed mechanisms typical for granular materials and laminates.

摘要

本文描述了TiSiC粉末的合成过程。研究了摩尔比和两种碳形态对所得粉末相组成的影响。合成过程采用放电等离子烧结（SPS）炉进行。此外，利用所得粉末制备了SiC颗粒增强复合材料。所得结果表明，碳形态对合成后粉末的纯度没有影响，而退火对其有显著影响。复合材料也在1300和1400℃两个温度下使用SPS炉进行固结。测试表明，1300℃烧结的复合材料密度和硬度较低（对于10%SiC增强复合材料，最大密度分别为3.97 g/cm³和硬度为447 HV5）。对于在1400℃烧结的复合材料（TiAlC-10%SiC，最大密度4.43 g/cm³和硬度1153 HV5），这些参数显著增加。此外，裂纹扩展分析显示了颗粒材料和层压板的典型机制。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/249f/9917825/171ef0edf644/materials-16-00889-g011a.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/249f/9917825/4d1b81b2f414/materials-16-00889-g001.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/249f/9917825/3496829ba77a/materials-16-00889-g002.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/249f/9917825/97946e6540fe/materials-16-00889-g003.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/249f/9917825/50ebf7556820/materials-16-00889-g004.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/249f/9917825/6118eb53f470/materials-16-00889-g005.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/249f/9917825/7b8428872b58/materials-16-00889-g006.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/249f/9917825/806d121309e9/materials-16-00889-g007.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/249f/9917825/154d5ad57fc2/materials-16-00889-g008.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/249f/9917825/7ba668eb2e02/materials-16-00889-g009.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/249f/9917825/8e19fbac4226/materials-16-00889-g010.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/249f/9917825/171ef0edf644/materials-16-00889-g011a.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/249f/9917825/4d1b81b2f414/materials-16-00889-g001.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/249f/9917825/3496829ba77a/materials-16-00889-g002.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/249f/9917825/97946e6540fe/materials-16-00889-g003.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/249f/9917825/50ebf7556820/materials-16-00889-g004.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/249f/9917825/6118eb53f470/materials-16-00889-g005.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/249f/9917825/7b8428872b58/materials-16-00889-g006.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/249f/9917825/806d121309e9/materials-16-00889-g007.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/249f/9917825/154d5ad57fc2/materials-16-00889-g008.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/249f/9917825/7ba668eb2e02/materials-16-00889-g009.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/249f/9917825/8e19fbac4226/materials-16-00889-g010.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/249f/9917825/171ef0edf644/materials-16-00889-g011a.jpg

相似文献

1
Synthesis of TiSiC Phases and Consolidation of MAX/SiC Composites-Microstructure and Mechanical Properties.TiSiC相的合成及MAX/SiC复合材料的固结——微观结构与力学性能
Materials (Basel). 2023 Jan 17;16(3):889. doi: 10.3390/ma16030889.
2
Structure and Deformation Behavior of Ti-SiC Composites Made by Mechanical Alloying and Spark Plasma Sintering.机械合金化和放电等离子烧结制备的Ti-SiC复合材料的结构与变形行为
Materials (Basel). 2019 Apr 18;12(8):1276. doi: 10.3390/ma12081276.
3
Microstructure and Mechanical Properties of Composites Obtained by Spark Plasma Sintering of TiSiC-15 vol.%Cu Mixtures.通过火花等离子烧结TiSiC-15体积%铜混合物获得的复合材料的微观结构和力学性能
Materials (Basel). 2022 Mar 29;15(7):2515. doi: 10.3390/ma15072515.
4
The Microstructure, Mechanical, and Friction-Wear Properties of Boron Carbide-Based Composites with TiB and SiC Formed In Situ by Reactive Spark Plasma Sintering.通过反应性放电等离子烧结原位形成的含TiB和SiC的碳化硼基复合材料的微观结构、力学性能及摩擦磨损性能
Materials (Basel). 2024 May 16;17(10):2379. doi: 10.3390/ma17102379.
5
Novel Alumina Matrix Composites Reinforced with MAX Phases-Microstructure Analysis and Mechanical Properties.MAX相增强的新型氧化铝基复合材料——微观结构分析与力学性能
Materials (Basel). 2022 Oct 5;15(19):6909. doi: 10.3390/ma15196909.
6
Sintering and Mechanical Properties of (SiC + TiC)/Fe Composites Synthesized from TiAlC, SiC, and Fe Powders.由TiAlC、SiC和铁粉合成的(SiC + TiC)/Fe复合材料的烧结及力学性能
Materials (Basel). 2021 May 9;14(9):2453. doi: 10.3390/ma14092453.
7
Processing and Characterization of Spark Plasma Sintered SiC-TiB-TiC Powders.放电等离子烧结SiC-TiB-TiC粉末的加工与表征
Materials (Basel). 2022 Mar 5;15(5):1946. doi: 10.3390/ma15051946.
8
Pulse Plasma Sintering of NiAl-AlO Composite Powder Produced by Mechanical Alloying with Contribution of Nanometric AlO Powder.机械合金化制备的NiAl-AlO复合粉末的脉冲等离子烧结及纳米AlO粉末的作用
Materials (Basel). 2022 Jan 6;15(2):407. doi: 10.3390/ma15020407.
9
Synthesis and Tribological Characterization of TiSiC/ZnO Composites.TiSiC/ZnO复合材料的合成与摩擦学表征
Materials (Basel). 2021 Oct 14;14(20):6088. doi: 10.3390/ma14206088.
10
Microstructure and Mechanical Properties of Low-Cost SiC-Reinforced Aluminum and Al4Cu Matrix Composites Produced by Sintering in Vacuum.通过真空烧结制备的低成本碳化硅增强铝及Al4Cu基复合材料的微观结构与力学性能
Materials (Basel). 2023 Aug 7;16(15):5492. doi: 10.3390/ma16155492.

引用本文的文献

1
Exploring semiconductor potential: novel boron-based TiAlC and TiAlN MAX phase composites with tunable band gaps.探索半导体潜力：具有可调带隙的新型硼基TiAlC和TiAlN MAX相复合材料
Nanoscale Adv. 2024 Nov 12;7(1):288-309. doi: 10.1039/d4na00738g. eCollection 2024 Dec 17.
2
Theoretical Prediction and Experimental Synthesis of ZrAC (A = Cd, Sb) Phases.ZrAC（A = Cd，Sb）相的理论预测与实验合成
Materials (Basel). 2024 Mar 28;17(7):1556. doi: 10.3390/ma17071556.
3
Effects of TiC, Si, and Al on Combustion Synthesis of TiSiC/TiC/TiSi Composites.

本文引用的文献

1
Novel Alumina Matrix Composites Reinforced with MAX Phases-Microstructure Analysis and Mechanical Properties.MAX相增强的新型氧化铝基复合材料——微观结构分析与力学性能
Materials (Basel). 2022 Oct 5;15(19):6909. doi: 10.3390/ma15196909.
2
Microstructure and Mechanical Properties of Alumina Composites with Addition of Structurally Modified 2D TiC (MXene) Phase.添加结构改性二维TiC（MXene）相的氧化铝复合材料的微观结构与力学性能
Materials (Basel). 2021 Feb 10;14(4):829. doi: 10.3390/ma14040829.
3
Influence of MXene (TiC) Phase Addition on the Microstructure and Mechanical Properties of Silicon Nitride Ceramics.
TiC、Si和Al对TiSiC/TiC/TiSi复合材料燃烧合成的影响。
Materials (Basel). 2023 Sep 9;16(18):6142. doi: 10.3390/ma16186142.
MXene（TiC）相添加对氮化硅陶瓷微观结构和力学性能的影响
Materials (Basel). 2020 Nov 19;13(22):5221. doi: 10.3390/ma13225221.