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塑性变形奥氏体高锰钢的显微硬度、压痕尺寸效应及真实硬度

Microhardness, Indentation Size Effect and Real Hardness of Plastically Deformed Austenitic Hadfield Steel.

作者信息

Luo Quanshun, Kitchen Matthew

机构信息

Materials and Engineering Research Institute, Sheffield Hallam University, Sheffield S1 1WB, UK.

出版信息

Materials (Basel). 2023 Jan 28;16(3):1117. doi: 10.3390/ma16031117.

Abstract

Microhardness testing is a widely used method for measuring the hardness property of small-scale materials. However, pronounced indentation size effect (ISE) causes uncertainties when the method is used to estimate the real hardness. In this paper, three austenitic Hadfield steel samples of different plastic straining conditions were subjected to Vickers microhardness testing, using a range of loads from 10 to 1000 g. The obtained results reveal that the origin of ISE is derived from the fact, that the indentation load and the resultant indent diagonal do not obey Kick's law ( = · ). Instead, the and parameters obey Meyer's power law = ) with < 2. The plastically strained samples showed not only significant work hardening, but also different ISE significance, as compared to the non-deformed bulk steel. After extensive assessment of several theoretical models, including the Hays-Kendall model, Li-Bradt model, Bull model and Nix-Gao model, it was found that the real hardness can be determined by Vickers microhardness indentation and subsequent analysis using the Nix-Gao model. The newly developed method was subsequently utilised in two case studies to determine the real hardness properties of sliding worn surfaces and the subsurface hardness profile.

摘要

显微硬度测试是一种广泛用于测量小尺寸材料硬度特性的方法。然而,显著的压痕尺寸效应(ISE)使得该方法在用于估计实际硬度时产生不确定性。在本文中,对三种不同塑性应变条件的奥氏体哈德菲尔德钢样品进行了维氏显微硬度测试,使用的载荷范围为10至1000克。所得结果表明,ISE的起源在于压痕载荷和所得压痕对角线不遵循基克定律((p = k\cdot a))。相反,(p)和(a)参数遵循迈耶幂定律(p = C\cdot a^n),其中(n < 2)。与未变形的块状钢相比,经过塑性应变的样品不仅表现出显著的加工硬化,而且ISE的显著性也不同。在对包括海斯 - 肯德尔模型、李 - 布拉德模型、布尔模型和尼克斯 - 高模型在内的几种理论模型进行广泛评估后,发现可以通过维氏显微硬度压痕并随后使用尼克斯 - 高模型进行分析来确定实际硬度。随后,新开发的方法被用于两个案例研究,以确定滑动磨损表面的实际硬度特性和亚表面硬度分布。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/575c/9920888/afa61fb6cee9/materials-16-01117-g001.jpg

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