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热循环和消毒对 PETG/TPU 和 PMMA 的粗糙度、显微硬度和颜色的影响。

Influence of thermal cycles and disinfection on the roughness, microhardness and color of PETG/TPU and PMMA.

机构信息

Department of Dental Materials and Prosthodontics, School of Dentistry, São Paulo State University (UNESP), Araçatuba, Brazil.

出版信息

Polim Med. 2023 Jan-Jun;53(1):19-24. doi: 10.17219/pim/159350.

DOI:10.17219/pim/159350
PMID:36929643
Abstract

BACKGROUND

Occlusal splints can protect teeth during bruxism, preventing tooth wear, as well as during sports activities, shielding them from impacts.

OBJECTIVES

To verify the influence of thermal cycles and disinfection on the roughness, microhardness and color of polyethylene terephthalate glycol/thermoplastic polyurethane (PETG/TPU) and poly(methyl methacrylate) (PMMA).

MATERIAL AND METHODS

Thirty-six PETG/TPU samples and 36 PMMA samples were prepared (ø10 mm × 3 mm). Six groups were created according to the material and the disinfection method used (n = 12 each): PETG/TPU (glister), PETG/TPU (hypochlorite), PETG/TPU (soap), PMMA (glister), PMMA (hypochlorite), and PMMA (soap). Roughness, Knoop microhardness and color evaluations were performed before the experiments (T1), after thermocycling (T2) and after disinfection (T3). Three-way repeated measures analysis of variance (ANOVA) and Tukey's test were used for statistical evaluations.

RESULTS

For roughness and color, ANOVA showed statistical significance based on the interaction between thermal cycling, material and disinfectant factors. In terms of Knoop microhardness, ANOVA showed statistical significance based on the interaction between thermal cycling and material factors.

CONCLUSIONS

Roughness results were clinically acceptable in all groups at all time points, except the PETG/TPU and PMMA groups disinfected with hypochlorite. Microhardness significantly increased for both materials after thermal cycling, and at all time points, the microhardness of PMMA was significantly higher than that of PETG/TPU. After thermal cycling, the color changes were clinically unacceptable in all groups.

摘要

背景

咬合夹板在磨牙症期间可以保护牙齿,防止牙齿磨损,同时在运动期间也可以起到保护作用,防止受到冲击。

目的

验证热循环和消毒对聚对苯二甲酸乙二醇酯/热塑性聚氨酯(PETG/TPU)和聚甲基丙烯酸甲酯(PMMA)的粗糙度、显微硬度和颜色的影响。

材料和方法

制备 36 个 PETG/TPU 样本和 36 个 PMMA 样本(ø10 毫米×3 毫米)。根据使用的材料和消毒方法创建了 6 个组(每组 n = 12):PETG/TPU(glister)、PETG/TPU(次氯酸盐)、PETG/TPU(肥皂)、PMMA(glister)、PMMA(次氯酸盐)和 PMMA(肥皂)。在实验前(T1)、热循环后(T2)和消毒后(T3)进行粗糙度、努普显微硬度和颜色评估。使用三因素重复测量方差分析(ANOVA)和 Tukey 检验进行统计评估。

结果

对于粗糙度和颜色,ANOVA 显示基于热循环、材料和消毒剂因素的相互作用有统计学意义。在努普显微硬度方面,ANOVA 显示基于热循环和材料因素的相互作用有统计学意义。

结论

除了用次氯酸盐消毒的 PETG/TPU 和 PMMA 组外,所有组在所有时间点的粗糙度结果均在临床可接受范围内。经过热循环后,两种材料的显微硬度均显著增加,并且在所有时间点,PMMA 的显微硬度均显著高于 PETG/TPU。经过热循环后,所有组的颜色变化均在临床不可接受范围内。

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