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TiO纳米润滑剂对不锈钢SUS301微深冲影响的分析

Analysis of TiO Nanolubricant Influence in Micro Deep Drawing of Stainless Steel SUS301.

作者信息

Pan Di, Zhang Guangqing, Jia Fanghui, Li Lianjie, Zhang Tao, Lu Yao, Wu Hui, Yang Ming, Jiang Zhengyi

机构信息

School of Mechanical, Materials, Mechatronic and Biomedical Engineering, University of Wollongong, Northfields Ave., Wollongong, NSW 2522, Australia.

Graduate School of System Design, Tokyo Metropolitan University, Tokyo 191-0065, Japan.

出版信息

Materials (Basel). 2023 Mar 9;16(6):2196. doi: 10.3390/ma16062196.

Abstract

To improve the quality of products produced from microforming, various nanolubricants have been applied in the field of micromanufacturing in recent years. In this paper, the effects of glycerol-based lubricant containing TiO NPs (NPs) on micro deep drawing (MDD) of austenitic stainless steel (ASS) SUS301 were studied, and the lubrication mechanism involved was discussed. The MDD experiments were conducted with the SUS301 foils under dry, 1, 2, and 4 wt% TiO NP lubrication conditions. The results show that the use of the TiO nanolubricants can significantly improve the quality of the drawn cups in terms of decreased wrinkling and surface roughness. Besides, the concentration of TiO NPs influences lubricity by reducing friction during the MDD process. The peak drawing force is the lowest when 2 wt% nanolubricant is applied, which drops to 72.54 N from 77.38 N under dry conditions. The micro cup drawn under 2 wt% TiO nanolubricant has the best quality among those obtained under all the lubrication conditions. The lubrication mechanisms are derived from the mending effects of TiO NPs and the formation of thin lubricant films associated with the open lubricant pockets (OLPs) and close lubricant pocket (CLPs) theory in the MDD. The CLPs function as reservoirs that retain lubricants to counteract the load pressure, whereas the OLPs lead to lubricant leakage due to the higher flow resistance. It was found that the lubricant film and NPs are insufficient at a low concentration (1 wt%), while the lubrication performance can be enhanced with increased NP concentration. However, there exist apparent agglomerations on the surface of the produced micro cup when using 4 wt% nanolubricant, which greatly deteriorates the lubricant performance in the MDD process. It is concluded that the lubricant containing 2 wt% TiO NPs demonstrates the best lubrication performance during the MDD of ASS SUS301.

摘要

为提高微成形产品的质量,近年来各种纳米润滑剂已应用于微制造领域。本文研究了含TiO纳米颗粒(NPs)的甘油基润滑剂对奥氏体不锈钢(ASS)SUS301微深冲(MDD)的影响,并探讨了其中涉及的润滑机制。在干燥、1 wt%、2 wt%和4 wt% TiO NP润滑条件下,对SUS301箔材进行了MDD实验。结果表明,使用TiO纳米润滑剂可显著提高拉深杯的质量,减少起皱和表面粗糙度。此外,TiO NPs的浓度通过降低MDD过程中的摩擦力来影响润滑性。当施加2 wt%纳米润滑剂时,峰值拉深力最低,从干燥条件下的77.38 N降至72.54 N。在2 wt% TiO纳米润滑剂下拉深的微杯在所有润滑条件下质量最佳。润滑机制源于TiO NPs的修补作用以及与MDD中开放润滑腔(OLPs)和封闭润滑腔(CLPs)理论相关的薄润滑膜的形成。CLPs起到储存润滑剂以抵抗负载压力的作用,而OLPs由于较高的流动阻力导致润滑剂泄漏。研究发现,在低浓度(1 wt%)时,润滑膜和NPs不足,而随着NP浓度的增加,润滑性能可得到增强。然而,使用4 wt%纳米润滑剂时,所生产微杯表面存在明显团聚,这在很大程度上恶化了MDD过程中的润滑性能。得出的结论是,含2 wt% TiO NPs的润滑剂在ASS SUS301的MDD过程中表现出最佳润滑性能。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/4832/10054133/dcfea18cd99f/materials-16-02196-g001.jpg

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