Darwich Rama A, Awad Manal, Abou Neel Ensanya A
Preventive and Restorative Dentistry Department, College of Dental Medicine, University of Sharjah, Sharjah P.O. Box 27272, United Arab Emirates.
UCL Eastman Dental Institute, Biomaterials & Tissue Engineering, Royal Free Hospital, Rowland and Hill Street, London NW3 2QG, UK.
Materials (Basel). 2023 Mar 15;16(6):2356. doi: 10.3390/ma16062356.
This study aimed to evaluate the effect of seven different decontamination methods (water, ZirClean, 37% phosphoric acid, 9.5% hydrofluoric acid, AlO sandblasting, low-speed dental stone, and high-speed dental stone) on the fracture resistance, microstructure, and surface roughness of monolithic and multilayered zirconia. The as-received and sandblasted zirconia was used as a control. One-way ANOVA and -test were performed. As-received monolithic zirconia was stronger (856 ± 94 MPa) than multilayered zirconia (348.4 ± 63 MPa). Only phosphoric acid (865 ± 141 MPa) and low-speed dental stone (959 ± 116 MPa) significantly increased the flexural strength of sandblasted monolithic zirconia (854 ± 99 MPa), but all tested decontamination methods except phosphoric acid (307 ± 57 MPa) and AlO (322 ± 69 MPa) significantly increased the flexural strength of sandblasted multilayered zirconia (325 ± 74 MPa). Different decontamination methods did not significantly affect the flexural modulus, but introduced irregularities in the crystal as well as deep surface flaws in both types of zirconia. The surface of sandblasted monolithic zirconia is more resistant to change than multilayered zirconia. Among different decontamination methods, a low-speed dental stone could be beneficial as it significantly increased the surface roughness and fracture resistance of both types of zirconia.
本研究旨在评估七种不同的去污方法(水、ZirClean、37%磷酸、9.5%氢氟酸、AlO喷砂、低速牙科用石膏和高速牙科用石膏)对整体式和多层氧化锆的抗断裂性、微观结构及表面粗糙度的影响。将原样接收的和经过喷砂处理的氧化锆用作对照。进行了单因素方差分析和t检验。原样接收的整体式氧化锆(856±94兆帕)比多层氧化锆(348.4±63兆帕)更强。只有磷酸(865±141兆帕)和低速牙科用石膏(959±116兆帕)显著提高了喷砂处理的整体式氧化锆(854±99兆帕)的抗弯强度,但除了磷酸(307±57兆帕)和AlO(322±69兆帕)外,所有测试的去污方法均显著提高了喷砂处理的多层氧化锆(325±74兆帕)的抗弯强度。不同的去污方法对弯曲模量没有显著影响,但在两种类型的氧化锆中均导致了晶体不规则以及表面深层缺陷。喷砂处理的整体式氧化锆表面比多层氧化锆更耐变化。在不同的去污方法中,低速牙科用石膏可能有益,因为它显著增加了两种类型氧化锆的表面粗糙度和抗断裂性。