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微波辅助从菠萝蜜残渣中提取果胶:优化、理化性质及抗菌活性

Microwave-assisted extraction of pectin from jackfruit rags: Optimization, physicochemical properties and antibacterial activities.

作者信息

Tran Ngan Thi Kim, Nguyen Viet Bao, Tran Thuan Van, Nguyen Thuy Thi Thanh

机构信息

Nong Lam University Ho Chi Minh City, Ho Chi Minh City 700000, Viet Nam.

Institute of Applied Technology and Sustainable Development, Nguyen Tat Thanh University, 298-300A Nguyen Tat Thanh, District 4, Ho Chi Minh City 755414, Viet Nam.

出版信息

Food Chem. 2023 Aug 30;418:135807. doi: 10.1016/j.foodchem.2023.135807. Epub 2023 Mar 7.

DOI:10.1016/j.foodchem.2023.135807
PMID:36989643
Abstract

While fruit biowastes pose an environmental hazard, they can be utilized as a source of beneficial biopolymers such as pectin. However, conventional extraction techniques require long processing time with low, impure yields, and microwave assisted extraction (MAE) can suffer from these drawbacks. Here, MAE was applied to extract pectin from jackfruit rags and compared with conventional heating reflux extraction (HRE). Response surface methodology was adopted to optimize pectin yield, based on pH (1.0-2.0), solid-liquid ratio (1:20-1:30), time (5-90 min), and temperature (60-95 °C). Pectin extraction by MAE required lower temperatures (65.99 °C) and shorter reaction times (10.56 min). Pectin HRE resulted in a product with amorphous structures and rough surfaces, while pectin-MAE was high crystalline with smooth surfaces. Although both pectin samples showed shear-thinning behavior, pectin-MAE exhibited higher antioxidant and antibacterial activities. Therefore, microwave assisted extraction was an efficient method to extract pectin from jackfruit rags.

摘要

虽然水果生物废料会对环境造成危害,但它们可以用作有益生物聚合物(如果胶)的来源。然而,传统的提取技术需要较长的处理时间,且产量低、纯度不高,微波辅助提取(MAE)也可能存在这些缺点。在此,采用微波辅助提取从菠萝蜜残渣中提取果胶,并与传统加热回流提取(HRE)进行比较。基于pH值(1.0 - 2.0)、固液比(1:20 - 1:30)、时间(5 - 90分钟)和温度(60 - 95℃),采用响应面法优化果胶产量。微波辅助提取果胶所需温度较低(65.99℃),反应时间较短(10.56分钟)。加热回流提取得到的果胶产品结构无定形且表面粗糙,而微波辅助提取的果胶结晶度高且表面光滑。虽然两种果胶样品均表现出剪切变稀行为,但微波辅助提取的果胶具有更高的抗氧化和抗菌活性。因此,微波辅助提取是从菠萝蜜残渣中提取果胶的有效方法。

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