Abdulrazzaq Ruba Husam, Hussein Basima Mohammed Ali
Department of Biomedical Applications, Institute of Laser for Postgraduate Studies, University of Baghdad, Baghdad, Iraq.
J Lasers Med Sci. 2022 Dec 27;13:e77. doi: 10.34172/jlms.2022.77. eCollection 2022.
The present study was performed to evaluate the influence of a 1064 nm fiber laser on shear bond strength (SBS) at the interface of titanium and resin cement. Forty titanium discs of 6 mm × 3 mm (diameter and thickness respectively) were categorized into four groups (n=10): control group without any surface treatment and three groups treated with a fiber laser with 81 ns pulse duration, 30 kHz frequency, 10000 mm/s scanning speed, 0.05 mm spot size, and different average power values (3, 5 and 7 W) depending on the tested group. Titanium disc characterization was performed by the scanning electron microscope (SEM) and surface roughness tester. Phase analysis was achieved using an X-ray diffractometer (XRD). Following these tests, resin cement application to titanium discs was performed. SBS values were determined by the universal testing machine. After debonding, the surface of titanium discs was examined by the stereomicroscope for the determination of failure modes. Data analysis was performed using analysis of variance (ANOVA) and Tukey HSD tests (α=0.05). A higher surface roughness value was observed in the 7 W group followed by the 5 W and 3 W groups, and the lowest surface roughness was in the control group. Additionally, the lowest SBS value was obtained from the control group and the highest SBS value was obtained from the 7 W group followed by the 5 W and 3 W groups. SBS between titanium abutment and resin cement can be significantly enhanced by using a fiber laser as a surface treatment considering tested laser parameters; additionally, a positive association between surface roughness and SBS was noted in the experimental groups.
本研究旨在评估1064纳米光纤激光对钛与树脂水门汀界面剪切粘结强度(SBS)的影响。将40个直径6毫米、厚度3毫米的钛盘分为四组(n = 10):未进行任何表面处理的对照组,以及三组分别用脉冲持续时间81纳秒、频率30千赫兹、扫描速度10000毫米/秒、光斑尺寸0.05毫米且平均功率值不同(根据测试组分别为3瓦、5瓦和7瓦)的光纤激光进行处理的组。通过扫描电子显微镜(SEM)和表面粗糙度测试仪对钛盘进行表征。使用X射线衍射仪(XRD)进行相分析。在这些测试之后,将树脂水门汀应用于钛盘。通过万能试验机测定SBS值。脱粘后,用立体显微镜检查钛盘表面以确定失效模式。使用方差分析(ANOVA)和Tukey HSD检验(α = 0.05)进行数据分析。观察到7瓦组的表面粗糙度值最高,其次是5瓦组和3瓦组,对照组的表面粗糙度最低。此外,对照组获得的SBS值最低,7瓦组获得的SBS值最高,其次是5瓦组和3瓦组。考虑到测试的激光参数,使用光纤激光作为表面处理可显著提高钛基台与树脂水门汀之间的SBS;此外,在实验组中还注意到表面粗糙度与SBS之间存在正相关。