Sayyar Navid, Hansen Vidar, Tucho Wakshum Mekonnen, Minde Mona Wetrhus
Department of Mechanical and Structural Engineering and Materials Science, University of Stavanger, 4036 Stavanger, Norway.
Heliyon. 2023 Apr 1;9(4):e15144. doi: 10.1016/j.heliyon.2023.e15144. eCollection 2023 Apr.
Microstructure and texture evolution of directed-laser deposited super-duplex stainless-steel, in the as-received block, were characterized using light and electron microscopies and electron backscattered diffraction. Mechanical properties in different directions were studied. Local FCC-depleted and FCC-rich zones and extensive precipitation of oxides were detected at the matrix wherein the different types of reformed austenite were surrounded by the elongated coarse ferrite. A vertical gradient of austenite content, caused by overall change in cooling rate, generated a waning hardness distribution along the building direction. The texture of austenite across the different deposition layers was not as intense as that of the ferrite. A dominant ⫽ND fibre, embedding strong Cube , was calculated for ferrite on the layer away from the bottom while the Goss appeared in the layer near the building substrate due to the considerable epitaxially developed grains. The less intensified multi-component texture of austenite at the layer near the substrate changed to ⫽ND fibre adorned by Rotated-Goss and Goss components at the upper layers where an incomplete fibre with a major Rotated-Cube was also partially inherited from the parent phase. The inter-phase boundaries obeying Kurdjumov-Sachs orientation relationship were predominantly formed at all layers. A slight increase of Σ3 coincidence site lattice interfaces was observed in austenite across the build direction. The possible mechanical anisotropy was depressed due to complex and multi-component transformation texture of the austenite. The material showed brittleness corresponding to significantly high tensile strength and low impact toughness.
采用光学显微镜、电子显微镜和电子背散射衍射对直接激光沉积的超级双相不锈钢铸态坯料的微观结构和织构演变进行了表征。研究了不同方向的力学性能。在基体中检测到局部贫FCC区和富FCC区以及大量氧化物析出,其中不同类型的再结晶奥氏体被拉长的粗大铁素体包围。冷却速率的整体变化导致奥氏体含量的垂直梯度,从而在堆积方向上产生硬度递减分布。不同沉积层上奥氏体的织构不如铁素体强烈。对于远离底部的层上的铁素体,计算出一个占主导地位的⫽ND纤维,其中嵌入了较强的立方织构,而由于大量外延生长的晶粒,高斯织构出现在靠近堆积基板的层中。靠近基板的层上奥氏体强度较低的多组分织构在上层转变为⫽ND纤维,由旋转高斯织构和高斯织构组分修饰,其中一个主要为旋转立方织构的不完整纤维也部分继承自母相。在所有层中主要形成了符合库尔久莫夫-萨克斯取向关系的相界。在整个堆积方向上,奥氏体中观察到Σ3重合点阵界面略有增加。由于奥氏体复杂的多组分转变织构,材料的可能机械各向异性得到了抑制。该材料表现出脆性,对应着显著较高的抗拉强度和较低的冲击韧性。