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阳离子淀粉-黄原胶复合纳米粒子的制备及乳化性能。

Preparation and emulsification properties of cationic starch-xanthan gum composite nanoparticles.

机构信息

School of Food Science, Guangdong Pharmaceutical University, Zhongshan, Guangdong Province 528458, China; GDPU-HKU Zhongshan Biomedical Innovation Platform, Zhongshan, Guangdong Province 528458, China.

School of Food Science, Guangdong Pharmaceutical University, Zhongshan, Guangdong Province 528458, China; GDPU-HKU Zhongshan Biomedical Innovation Platform, Zhongshan, Guangdong Province 528458, China.

出版信息

Food Chem. 2023 Sep 30;421:136143. doi: 10.1016/j.foodchem.2023.136143. Epub 2023 Apr 18.

Abstract

In this work, nanoparticles were prepared by the composite of cationic starch (CS) and xanthan gum (XG) through gelatinization and alcohol precipitation for the first time. Physicochemical properties, micromorphology, and emulsification properties of CS/XG nanoparticles were measured. SEM showed that after compositing with XG, the diameter size of the CS/XG nanoparticles was increased from about 50 nm to 150-300 nm. FT-IR, XRD and C CP/MAS NMR confirmed that XG was successfully complexed with CS. Besides, the visual observation indicated emulsions stabilized by CS/XG nanoparticles had excellent storage and thermal properties. Additionally, the rheological and stability results of emulsions show that pH and NaCl had effects on the rheological and stability properties of emulsions, which means that the prepared emulsions had environmental responsiveness. Thus, this work provides an efficient method to prepare CS and GX composite nanoparticles with efficient emulsifying properties.

摘要

在这项工作中,首次通过糊化和醇沉法将阳离子淀粉(CS)和黄原胶(XG)复合制备纳米颗粒。测量了 CS/XG 纳米颗粒的物理化学性质、微观形态和乳化性能。SEM 表明,与 XG 复合后,CS/XG 纳米颗粒的直径尺寸从约 50nm 增加到 150-300nm。FT-IR、XRD 和 C CP/MAS NMR 证实 XG 已成功与 CS 复合。此外,目视观察表明,由 CS/XG 纳米颗粒稳定的乳液具有优异的储存和热稳定性。此外,乳液的流变和稳定性结果表明,pH 和 NaCl 对乳液的流变和稳定性特性有影响,这意味着所制备的乳液具有环境响应性。因此,这项工作提供了一种有效的方法来制备具有高效乳化性能的 CS 和 GX 复合纳米颗粒。

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