Cuzic Cristiana, Jivanescu Anca, Negru Radu Marcel, Hulka Iosif, Rominu Mihai
Department of Prosthodontics, Faculty of Dental Medicine, University of Medicine and Pharmacy "Victor Babes", 300041 Timisoara, Romania.
Research Center of Digital and Advanced Technique for Endodontic, Restorative, and Prosthetic Treatment (TADERP), 300041 Timisoara, Romania.
Materials (Basel). 2023 Jun 10;16(12):4303. doi: 10.3390/ma16124303.
All-ceramic restorations are the foundation of modern esthetic dentistry. Clinical approaches for preparation, durability, aesthetics, and repair have been reformed by the idea of adhesive dentistry. The aim of the study and the objective question was to evaluate the impact of heated hydrofluoric acid pretreatment and the application technique's influence on the surface morphology and roughness of leucite-reinforced glass-ceramic materials (IPS Empress CAD, Ivoclar Vivadent), which is fundamental for understanding the adhesive cementation process. Scanning electron microscopy was used to observe the effectiveness of the two HF (Yellow Porcelain Etch, Cerkamed) application techniques and the HF's temperature impact on the surface topography of the ceramic. Based on surface conditioning methods, the adhesive cement (Panavia V5, Kuraray Noritake Dental Inc., Tokyo, Japan) was applied to the conditioned ceramic samples and light-cured. Shear bond strength values were correlated with the micro-retentive surface texture of the ceramic. With universal testing equipment at a 0.5 mm/min crosshead speed, SBS values between the resin cement and the ceramic material were assessed until failure. Analyzing the fractured surfaces of the specimens by digital microscopy, the failure modes were divided into three categories: adhesive, cohesive, and mixed failure. Analysis of variance (ANOVA) was used to statistically analyze the collected data. The results show that alternative treatment methods affected the material's surface characteristics and have an influence on the shear bond strength.
全瓷修复体是现代美学牙科的基础。粘结牙科理念革新了修复体预备、耐久性、美学效果及修复方面的临床方法。本研究的目的及核心问题是评估加热氢氟酸预处理及其应用技术对白榴石增强型玻璃陶瓷材料(义获嘉全瓷CAD,义获嘉伟瓦登特公司)表面形态和粗糙度的影响,这对于理解粘结固位过程至关重要。采用扫描电子显微镜观察两种氢氟酸(黄瓷蚀刻剂,Cerkamed)应用技术的效果以及氢氟酸温度对陶瓷表面形貌的影响。基于表面处理方法,将粘结剂(帕娜碧亚V5,可乐丽诺瑞特牙科公司,日本东京)应用于处理后的陶瓷样本并进行光固化。剪切粘结强度值与陶瓷的微固位表面纹理相关。使用万能测试设备以0.5毫米/分钟的横梁速度评估树脂粘结剂与陶瓷材料之间的SBS值直至破坏。通过数码显微镜分析样本的断裂表面,将破坏模式分为三类:粘结破坏、内聚破坏和混合破坏。采用方差分析(ANOVA)对收集的数据进行统计学分析。结果表明,替代处理方法影响了材料的表面特性并对剪切粘结强度有影响。