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采用响应面法优化废机油制备低粘度橡胶沥青的参数。

Optimizing parameters for the preparation of low viscosity rubber asphalt incorporating waste engine oil using response surface methodology.

机构信息

School of Civil and Architectural Engineering, Xi'an University of Science and Technology, Xi'an, 710054, China.

Road Engineering Research Center, Xi'an University of Science and Technology, Xi'an, 710054, China.

出版信息

Environ Sci Pollut Res Int. 2023 Aug;30(37):87433-87448. doi: 10.1007/s11356-023-28383-2. Epub 2023 Jul 8.

Abstract

Due to the high viscosity, rubber asphalt displays poor construction workability, which ultimately compromises the comfort and safety of pavement. In this study, specified control variates were used to study the effect of the waste engine oil (WEO) addition sequence on the properties of rubber asphalt while ensuring the consistency of other preparation parameters. Initially, in order to evaluate their compatibility, the storage stability and aging properties of the three groups of samples were determined. The variation of asphalt viscosity was then analyzed using a low-field nuclear magnetic resonance (LF-NMR) test, by predicting the fluidity of each sample. Subsequently, the results showed that the rubber asphalt prepared by premixing WEO and crumb rubber (CR) had the best properties of low temperature, compatibility, and fluidity. On this basis, the effects of WEO content, shear rate, shear temperature, and shear time on the properties of low viscosity rubber asphalt were investigated separately through response surface methodology (RSM). Quantitative data from the basic performance experiment were used to fit the high precision regression equation, thereby correlating a more precise level of factors with experimental results. The response surface model prediction analysis showed that the optimal preparation parameters of the low viscosity rubber asphalt were 60 min shear time, 180 °C shear temperature, and 5000 r/min shear rate. Simultaneously, the addition of 3.5% of WEO showed great potential as an asphalt viscosity reducer. Ultimately, this study provides an accurate method for determining the optimum preparation parameters of asphalt.

摘要

由于高粘度,橡胶沥青表现出较差的施工工艺性,最终会影响路面的舒适性和安全性。在本研究中,使用特定的控制变量来研究废发动机油(WEO)添加顺序对橡胶沥青性能的影响,同时确保其他制备参数的一致性。首先,为了评估它们的相容性,测定了三组样品的贮存稳定性和老化性能。然后,通过低场核磁共振(LF-NMR)试验分析了沥青粘度的变化,预测了每个样品的流动性。随后的结果表明,通过预混合 WEO 和胶粉(CR)制备的橡胶沥青具有最佳的低温、相容性和流动性性能。在此基础上,通过响应面法(RSM)分别研究了 WEO 含量、剪切速率、剪切温度和剪切时间对低粘度橡胶沥青性能的影响。基本性能实验的定量数据用于拟合高精度回归方程,从而将更精确的因素水平与实验结果相关联。响应面模型预测分析表明,低粘度橡胶沥青的最佳制备参数为剪切时间 60min、剪切温度 180°C 和剪切速率 5000r/min。同时,添加 3.5%的 WEO 作为沥青粘度降低剂具有很大的潜力。最终,本研究为确定沥青的最佳制备参数提供了一种准确的方法。

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