Osman Mahmoud, Sarafan Sheida, Wanjara Priti, Bernier Fabrice, Atabay Sila Ece, Gholipour Javad, Molavi-Zarandi Marjan, Soost Josh, Brochu Mathieu
National Research Council Canada, Montréal, QC H3T 1J4, Canada.
Department of Mining and Materials Engineering, McGill University, Montréal, QC H3A 0C5, Canada.
Materials (Basel). 2023 Jun 30;16(13):4749. doi: 10.3390/ma16134749.
The present work investigates the effectiveness of two heat treatment cycles-solution treatment + aging (STA) and direct aging (DA)-on optimizing the microstructure and enhancing the mechanical properties of 18Ni-300 maraging steel (300 MS) produced by additive-subtractive hybrid manufacturing (ASHM). The STA treatment led to a fully martensitic microstructure with minor remnants of the cellular substructures associated with the solidification conditions in ASHM. DA resulted in some reverted austenite and partial dissolution of the cellular morphologies into shorter fragments. Despite the contrasting microstructures, the tensile strength and the macro- and micro-hardness were comparable between STA and DA conditions. By contrast, the potential for improving the ductility was higher with the DA heat treatment. This is attributed to the higher reverted austenite content in the samples treated by DA, i.e., up to a maximum of 13.4% compared to less than 3.0% in the STA samples. For the DA sample with the highest reverted austenite content of 13.4%, the highest local and global fracture strain values of 30.1 and 5.9 ± 0.6% were measured, while the respective values were 23.4 and 4.4 ± 0.1% for the corresponding STA sample. This work suggests that DA of 300 MS produced by ASHM is sufficient to achieve comparable hardness and tensile strength to STA, whilst maintaining reasonable ductility. Avoiding the solution treatment cycle, with its appreciably higher temperatures, could benefit the dimensional stability and surface quality that are important for ASHM of 300 MS parts.
本研究探讨了两种热处理循环——固溶处理+时效处理(STA)和直接时效处理(DA)——对优化通过增减材混合制造(ASHM)生产的18Ni-300马氏体时效钢(300 MS)的微观结构和提高其力学性能的有效性。STA处理导致形成完全马氏体微观结构,其中残留少量与ASHM凝固条件相关的胞状亚结构。DA处理导致出现一些逆转变奥氏体,并且胞状形态部分溶解为较短的片段。尽管微观结构存在差异,但STA和DA条件下的抗拉强度以及宏观和微观硬度相当。相比之下,DA热处理提高延展性的潜力更大。这归因于DA处理样品中逆转变奥氏体含量较高,即最高可达13.4%,而STA样品中该含量小于3.0%。对于逆转变奥氏体含量最高达13.4%的DA样品,测得的局部和整体断裂应变值分别为30.1%和5.9±0.6%,而相应的STA样品的这些值分别为23.4%和4.4±0.1%。这项工作表明,对由ASHM生产的300 MS进行DA处理足以获得与STA相当的硬度和抗拉强度,同时保持合理的延展性。避免固溶处理循环(其温度明显更高)可能有利于尺寸稳定性和表面质量,这对于300 MS零件的ASHM很重要。