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[空气中甲醛测定的极谱法]

[Polarographic method of determining formaldehyde in air].

作者信息

Koen E, Ivanov G

出版信息

Probl Khig. 1979;4:50-62.

PMID:37500
Abstract

A rapid polarographic method for determination of formaldehyde microconcentrations in air has been developed. The method is highly sensitive - 0,5 cg/ml, which is 10 times higher than the sensitivity of the known methods now at use, with standard deviation less than 1.0. It is formaldehyde-selective - other saturated and unsaturated aldehydes, ketones, phenol, furfurol etc. do not interfere the determination. Sampling takes 15-20 min, polarographic analysis - 1 to 2 min. The method has been tested under conditions of production and proved to be highly reproducible and comparable with the colorimetric chromotropic acid technique.

摘要

已开发出一种用于测定空气中微量甲醛的快速极谱法。该方法灵敏度极高——为0.5微克/毫升,比目前使用的已知方法的灵敏度高10倍,标准偏差小于1.0。它对甲醛具有选择性——其他饱和与不饱和醛、酮、苯酚、糠醛等不干扰测定。采样需15 - 20分钟,极谱分析需1至2分钟。该方法已在生产条件下进行测试,结果表明具有高度可重复性,且与比色变色酸技术相当。

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