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高光谱相机在直线等离子体装置PSI-2上用于原位等离子体-材料相互作用研究的应用。

Application of a hyperspectral camera for in situ plasma-material interaction studies at the linear plasma device PSI-2.

作者信息

Li Changjun, Brezinsek Sebastijan, Ertmer Stephan, Kreter Arkadi, Reinhart Michael, Ding Rui, Chen Junling

机构信息

Institute of Plasma Physics, Chinese Academy of Sciences, Hefei 230031, People's Republic of China.

Forschungszentrum Jülich GmbH-Institut für Energie- und Klimaforschung-Plasmaphysik, Partner of the Trilateral Euregio Cluster (TEC), 52425 Jülich, Germany.

出版信息

Rev Sci Instrum. 2023 Aug 1;94(8). doi: 10.1063/5.0155722.

DOI:10.1063/5.0155722
PMID:37526517
Abstract

A hyperspectral camera (HSC-type Specim IQ) has been applied at the linear plasma device PSI-2 under steady-state conditions. The camera has the capacity of hyperspectral imaging (HSI) with the dimension of a data array 512 × 512 × 204 (x, y, λ) covering the spectral span from 400 to 1000 nm with moderate average spectral resolution (FWHM ∼7 nm). After radiometric calibration and background/continuum emission subtraction, two main applications of the camera, (i) plasma diagnostics in helium (He) plasmas and (ii) plasma-material interaction studies with tungsten (W) targets in neon (Ne) plasmas, have been carried out. The measurements were complemented by a movable Langmuir double probe system (LP) measuring electron temperature (Te) and electron density (ne) in radial direction r and a fiber-coupled cross-dispersion spectrometer with high spectral resolution (Spectrelle) recording neutral He, W, and Ne emission lines over the full plasma column. (i) Two-dimensional (2D) imaging of Te and ne radial profiles in axial direction z of the He plasma column were for the first time obtained by the regression analysis of Te and ne (from LP) and six He I line ratios (from HSC). The spatially resolved plasma parameters covered in these studies range between Te ∼ 0.8-13.4 eV and ne ∼ 0.2 × 1018-3.9 × 1018 m-3 and permit a reconstruction of the plasma conditions in PSI-2 in 2D without LP perturbation. (ii) W sputtering was studied in situ in Ne plasmas exposing W target samples (negatively biased at 100 V) under perpendicular Ne plasma impact. Simultaneously, the 2D distributions of W (W I line at 429.5 nm) in front of the target and the 2D Ne plasma distribution (Ne I line at 703.2 nm) were recorded with complete spectral separation as confirmed by the Spectrelle spectrometer. This permits the simultaneous measurement of the neutral W penetration and its angular distribution induced in the sputtering process and of the impinging plasma distribution. The HSI technique offers, despite a few technical drawbacks, such as the moderate spectral resolution and poor time resolution, a new possibility to distinguish multiple emission lines from plasma and impurities and complements the portfolio of existing Optical Emission Spectroscopy techniques, providing a good compromise regarding spectral, spatial, and temporal resolution.

摘要

一台高光谱相机(HSC型Specim IQ)已应用于稳态条件下的线性等离子体装置PSI-2。该相机具备高光谱成像(HSI)能力,数据阵列维度为512×512×204(x、y、λ),覆盖400至1000纳米的光谱范围,平均光谱分辨率适中(半高宽约7纳米)。在进行辐射校准和背景/连续发射扣除后,开展了该相机的两项主要应用:(i)氦(He)等离子体中的等离子体诊断;(ii)氖(Ne)等离子体中钨(W)靶材的等离子体-材料相互作用研究。测量工作由一个可移动的朗缪尔双探针系统(LP)辅助进行,该系统在径向r测量电子温度(Te)和电子密度(ne),还有一台具有高光谱分辨率的光纤耦合交叉色散光谱仪(Spectrelle)记录整个等离子体柱上的中性He、W和Ne发射线。(i)通过对Te和ne(来自LP)以及六条He I线比值(来自HSC)进行回归分析,首次获得了He等离子体柱轴向z方向上Te和ne径向分布的二维(2D)成像。这些研究中涵盖的空间分辨等离子体参数范围为Te约0.8 - 13.4电子伏特,ne约0.2×10^18 - 3.9×10^18立方米^-3,并且能够在无LP扰动的情况下二维重建PSI-2中的等离子体条件。(ii)在垂直Ne等离子体冲击下,对暴露于W靶材样品(负偏压100伏)的Ne等离子体中的W溅射进行了原位研究。同时,用Spectrelle光谱仪证实,以完全的光谱分离记录了靶材前方W(429.5纳米处的W I线)的二维分布和Ne等离子体的二维分布(703.2纳米处的Ne I线)。这使得能够同时测量溅射过程中诱导的中性W渗透及其角分布以及入射等离子体分布。尽管高光谱成像(HSI)技术存在一些技术缺陷,如中等光谱分辨率和较差的时间分辨率,但它为区分来自等离子体和杂质的多条发射线提供了新的可能性,补充了现有发射光谱技术的组合,在光谱、空间和时间分辨率方面实现了良好的折衷。

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