Robbins J E, Ball M S, Williams S A
Anal Biochem. 1986 Aug 15;157(1):84-8. doi: 10.1016/0003-2697(86)90199-5.
The synthesis of coenzyme A thioesters of 13C-labeled acetate, propionate, succinate, and methyl malonate is described. The average yields were 94%. The 13C-NMR spectra were determined to provide a reference for the resonance positions of these metabolites. The synthesis of coenzyme thioesters of small-molecular-weight acids labeled with 13C has not been described previously, nor have the resonance positions been previously reported.
