Suppr超能文献

MEPROS - 用于多功能高频电子顺磁共振光谱仪的模块化电子顺磁共振操作软件。

MEPROS - Modular electron paramagnetic resonance operating software for multifunctional high-frequency EPR spectrometer.

作者信息

Šedivý Matúš, Santana Vinicius, Sojka Antonín, Laguta Oleksii, Neugebauer Petr

机构信息

Magneto-Optical and THz Spectroscopy, Central European Institute of Technology (CEITEC), Brno University of Technology (BUT), Czech Republic; Department of Microelectronics, Faculty of Electrical Engineering and Communication, Brno University of Technology, Czech Republic.

Magneto-Optical and THz Spectroscopy, Central European Institute of Technology (CEITEC), Brno University of Technology (BUT), Czech Republic.

出版信息

J Magn Reson. 2023 Oct;355:107556. doi: 10.1016/j.jmr.2023.107556. Epub 2023 Sep 12.

Abstract

We present a software solution developed in LabVIEW for a home-built High-Frequency Electron Paramagnetic Resonance (HF-EPR) spectrometer. A modular approach was applied to control the spectrometer subsystems and simplify the adaptation to hardware changes during the development. The solution implements measuring procedures for conventional Continuous Wave EPR (CW-EPR), Frequency-Swept EPR (FS-EPR), and Two-Dimensional EPR (2D-EPR) mapping, which are relevant in different cases. The software's automation capabilities were tested in several trial measurements to obtain CW-EPR spectra of Silicon Carbide doped by vanadium (SiC + V) at various temperatures and microwave frequencies, multi-frequency spectra via 2D-EPR mapping, and dense FS-EPR data of a lithium phthalocyanine crystal rotated in a magnetic field. Several prospective modifications of the software are discussed in the conclusion. A modular character allows the easy re-use of code portions in other experimental setups. The spectrometer and the software are currently deployed and utilized in a laboratory of EPR spectroscopy at Central European Institute of Technology (CEITEC) in Brno, and data obtained by it has been already used in a number of publications.

摘要

我们展示了一种在LabVIEW中开发的用于自制高频电子顺磁共振(HF-EPR)光谱仪的软件解决方案。采用模块化方法来控制光谱仪子系统,并简化开发过程中对硬件变化的适应性。该解决方案实现了传统连续波EPR(CW-EPR)、频率扫描EPR(FS-EPR)和二维EPR(2D-EPR)映射的测量程序,这些程序在不同情况下都很重要。通过多次试验测量测试了该软件的自动化功能,以获取不同温度和微波频率下钒掺杂碳化硅(SiC + V)的CW-EPR光谱、通过2D-EPR映射获得的多频光谱以及在磁场中旋转的锂酞菁晶体的密集FS-EPR数据。结论中讨论了该软件的几种潜在改进。模块化特性允许在其他实验设置中轻松重用代码部分。该光谱仪和软件目前已在布尔诺的中欧技术研究所(CEITEC)的EPR光谱实验室中部署和使用,并且通过它获得的数据已经在许多出版物中得到应用。

文献检索

告别复杂PubMed语法,用中文像聊天一样搜索,搜遍4000万医学文献。AI智能推荐,让科研检索更轻松。

立即免费搜索

文件翻译

保留排版,准确专业,支持PDF/Word/PPT等文件格式,支持 12+语言互译。

免费翻译文档

深度研究

AI帮你快速写综述,25分钟生成高质量综述,智能提取关键信息,辅助科研写作。

立即免费体验