Šedivý Matúš, Santana Vinicius, Sojka Antonín, Laguta Oleksii, Neugebauer Petr
Magneto-Optical and THz Spectroscopy, Central European Institute of Technology (CEITEC), Brno University of Technology (BUT), Czech Republic; Department of Microelectronics, Faculty of Electrical Engineering and Communication, Brno University of Technology, Czech Republic.
Magneto-Optical and THz Spectroscopy, Central European Institute of Technology (CEITEC), Brno University of Technology (BUT), Czech Republic.
J Magn Reson. 2023 Oct;355:107556. doi: 10.1016/j.jmr.2023.107556. Epub 2023 Sep 12.
We present a software solution developed in LabVIEW for a home-built High-Frequency Electron Paramagnetic Resonance (HF-EPR) spectrometer. A modular approach was applied to control the spectrometer subsystems and simplify the adaptation to hardware changes during the development. The solution implements measuring procedures for conventional Continuous Wave EPR (CW-EPR), Frequency-Swept EPR (FS-EPR), and Two-Dimensional EPR (2D-EPR) mapping, which are relevant in different cases. The software's automation capabilities were tested in several trial measurements to obtain CW-EPR spectra of Silicon Carbide doped by vanadium (SiC + V) at various temperatures and microwave frequencies, multi-frequency spectra via 2D-EPR mapping, and dense FS-EPR data of a lithium phthalocyanine crystal rotated in a magnetic field. Several prospective modifications of the software are discussed in the conclusion. A modular character allows the easy re-use of code portions in other experimental setups. The spectrometer and the software are currently deployed and utilized in a laboratory of EPR spectroscopy at Central European Institute of Technology (CEITEC) in Brno, and data obtained by it has been already used in a number of publications.
我们展示了一种在LabVIEW中开发的用于自制高频电子顺磁共振(HF-EPR)光谱仪的软件解决方案。采用模块化方法来控制光谱仪子系统,并简化开发过程中对硬件变化的适应性。该解决方案实现了传统连续波EPR(CW-EPR)、频率扫描EPR(FS-EPR)和二维EPR(2D-EPR)映射的测量程序,这些程序在不同情况下都很重要。通过多次试验测量测试了该软件的自动化功能,以获取不同温度和微波频率下钒掺杂碳化硅(SiC + V)的CW-EPR光谱、通过2D-EPR映射获得的多频光谱以及在磁场中旋转的锂酞菁晶体的密集FS-EPR数据。结论中讨论了该软件的几种潜在改进。模块化特性允许在其他实验设置中轻松重用代码部分。该光谱仪和软件目前已在布尔诺的中欧技术研究所(CEITEC)的EPR光谱实验室中部署和使用,并且通过它获得的数据已经在许多出版物中得到应用。