Wen Jinli, Wang Yue, Cao Weiyu, He Yanli, Sun Yining, Yuan Pengqiang, Sun Bowei, Yan Yiping, Qin Hongyan, Fan Shutian, Lu Wenpeng
Institute of Special Animal and Plant Sciences, Chinese Academy of Agricultural Sciences, Changchun 130112, China.
Foods. 2023 Sep 6;12(18):3345. doi: 10.3390/foods12183345.
wine is a low-alcoholic beverage brewed from with a unique flavor and sweet taste. In this study, the basic physicochemical indicators, color, organic acid, and volatile aroma components of wines made from the varieties 'Kuilv', 'Fenglv', 'Jialv', 'Wanlv', 'Xinlv', 'Pinglv', 'Lvbao', 'Cuiyu', 'Tianxinbao', and 'Longcheng No.2' were determined, and a sensory evaluation was performed. The findings show that 'Tianxinbao' produced the driest extract (49.59 g/L), 'Kuilv' produced the most Vitamin C (913.46 mg/L) and total phenols (816.10 mg/L), 'Jialv' produced the most total flavonoids (477.12 mg/L), and 'Cuiyu' produced the most tannins (4.63 g/L). We analyzed the color of the wines based on *** parameters and found that the 'Kuilv' and 'Longcheng No.2' wines had the largest * value (31.65), the 'Pinglv' wines had the greatest * value (2.88), and the 'Kuilv' wines had the largest * value (5.08) and C* value (5.66) of the ten samples. A total of eight organic acids were tested in ten samples via high-performance liquid chromatography (HPLC), and we found that there were marked differences in the organic acid contents in different samples ( < 0.05). The main organic acids were citric acid, quinic acid, and malic acid. The aroma description of a wine is one of the keys to its quality. A total of 51 volatile compounds were identified and characterized in ten samples with headspace gas chromatography-ion mobility spectrometry, including 24 esters, 12 alcohols, 9 aldehydes, 3 aldehydes, 2 terpenes, and 1 acid, with the highest total volatile compound content in 'Fenglv'. There were no significant differences in the types of volatile compounds, but there were significant differences in the contents ( < 0.05). An orthogonal partial least squares discriminant analysis (OPLS-DA) based on the odor activity value (OAV) showed that ethyl butanoate, ethyl pentanoate, ethyl crotonate, ethyl isobutyrate, butyl butanoate, 2-methylbutanal, ethyl isovalerate, and ethyl hexanoate were the main odorant markers responsible for flavor differences between all the wines. Sensory evaluation is the most subjective and effective way for consumers to judge wine quality. A quantitative descriptive analysis (QDA) of the aroma profiles of ten grapes revealed that the 'fruity' and 'floral' descriptors are the main and most essential parts of the overall flavor of wines. 'Tianxinbao' had the highest total aroma score. The flavor and quality of wines greatly depend on the type and quality of the raw material. Therefore, high-quality raw materials can improve the quality of wines. The results of the study provide a theoretical basis for improving the quality of wines and demonstrate the application prospects of HS-GC-IMS in detecting wine flavors.
葡萄酒是一种由[原料]酿造而成的低酒精饮料,具有独特的风味和甜味。本研究测定了‘奎绿’‘凤绿’‘佳丽酿’‘万绿’‘新绿’‘平绿’‘绿宝’‘翠玉’‘天辛宝’和‘龙城二号’等品种葡萄酒的基本理化指标、色泽、有机酸和挥发性香气成分,并进行了感官评价。结果表明,‘天辛宝’的干浸出物含量最高(49.59g/L),‘奎绿’的维生素C含量(913.46mg/L)和总酚含量(816.10mg/L)最高,‘佳丽酿’的总黄酮含量最高(477.12mg/L),‘翠玉’的单宁含量最高(4.63g/L)。基于[参数]分析了这些葡萄酒的色泽,发现‘奎绿’和‘龙城二号’葡萄酒的值最大(31.65),‘平绿’葡萄酒的值最大(2.88),‘奎绿’葡萄酒在十个样品中值最大(5.08),C值最大(5.66)。通过高效液相色谱法(HPLC)对十个样品中的八种有机酸进行了检测,发现不同样品中的有机酸含量存在显著差异(<0.05)。主要有机酸为柠檬酸、奎宁酸和苹果酸。葡萄酒的香气描述是其品质的关键之一。采用顶空气相色谱-离子迁移谱法在十个样品中鉴定并表征了51种挥发性化合物,包括24种酯类、12种醇类、9种醛类、3种酮类、2种萜类和1种酸类,‘凤绿’中挥发性化合物的总含量最高。挥发性化合物的种类没有显著差异,但含量存在显著差异(<0.05)。基于气味活性值(OAV)的正交偏最小二乘法判别分析(OPLS-DA)表明,丁酸乙酯、戊酸乙酯、巴豆酸乙酯、异丁酸乙酯、丁酸丁酯、2-甲基丁醛、异戊酸乙酯和己酸乙酯是所有这些葡萄酒风味差异的主要气味标记物。感官评价是消费者判断葡萄酒品质最主观且有效的方式。对十种葡萄的香气特征进行定量描述分析(QDA)表明,‘果香’和‘花香’描述词是葡萄酒整体风味的主要且最关键部分。‘天辛宝’的总香气得分最高。葡萄酒的风味和品质很大程度上取决于葡萄原料的种类和质量。因此,优质原料可以提高葡萄酒的品质。本研究结果为提高葡萄酒品质提供了理论依据,并展示了HS-GC-IMS在检测葡萄酒风味方面的应用前景。