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激光纹理化 Ti-6Al-7Nb 合金在生物医学中的应用:表面性能对纹理化参数的研究。

Laser textured Ti-6Al-7Nb alloy for biomedical applications: An investigation of texturing parameters on surface properties.

机构信息

Department of Mechanical Engineering, Yozgat Bozok University, Yozgat, Turkey.

Department of Mechanical Engineering, Dokuz Eylul University, Izmir, Turkey.

出版信息

Proc Inst Mech Eng H. 2023 Oct;237(10):1139-1153. doi: 10.1177/09544119231200537. Epub 2023 Sep 30.

DOI:10.1177/09544119231200537
PMID:37776151
Abstract

Surface texturing with a laser beam is an effective method for engraving on the surface of biomaterials. The four laser texturing parameters (scan speed, frequency, fill spacing, and pulse width) having five different values were associated with five different scanning strategies (scan direction), and a total of 25 texturing conditions were tested on the Ti-6Al-7Nb alloy surface. The surface roughness and wettability of the textures created with a 20 W nanosecond fiber laser with a wavelength of 1064 nm on the surface of Ti-6Al-7Nb biocompatible alloy were investigated. Laser texturing parameters were analyzed according to the lowest surface roughness and a hydrophilic surface by creating L25 orthogonal arrays. The surface roughness values ranged between 2 and 26 µm. The lowest surface roughness with a value of 2.21 µm was achieved when the texture was processed with a frequency of 150 kHz, a fill spacing of 0.02 mm, a scan speed of 800 mm/s, a pulse width of 250 ns, and a cross-hatch strategy of 0°/90°. Considering the wettability test results, it was revealed that most of the textured surfaces have super hydrophilic and hydrophilic characteristics except the surface with a contact angle of 92.93°. The relevant surface was textured with 75 kHz frequency, 1000 mm/s scan speed, 0.05 mm fill spacing, 200 ns pulse width, and 45°/-45° cross-hatch strategy.

摘要

采用激光束对生物材料表面进行纹理加工是一种有效的雕刻方法。将四个激光纹理加工参数(扫描速度、频率、填充间距和脉冲宽度)设置为五个不同的值,并与五个不同的扫描策略(扫描方向)相关联,总共在 Ti-6Al-7Nb 合金表面测试了 25 种纹理加工条件。在 Ti-6Al-7Nb 生物相容性合金表面使用波长为 1064nm 的 20W 纳秒光纤激光,研究了表面粗糙度和润湿性。通过创建 L25 正交数组,根据最低表面粗糙度和亲水表面分析激光纹理加工参数。表面粗糙度值在 2 到 26μm 之间。当纹理以 150kHz 的频率、0.02mm 的填充间距、800mm/s 的扫描速度、250ns 的脉冲宽度和 0°/90°的交叉策略进行加工时,表面粗糙度达到最低值 2.21μm。考虑到润湿性测试结果,除接触角为 92.93°的表面外,大多数纹理表面都具有超亲水和亲水特性。具有此接触角的相关表面采用 75kHz 频率、1000mm/s 扫描速度、0.05mm 填充间距、200ns 脉冲宽度和 45°/-45°交叉策略进行纹理加工。

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