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含纳米级偏磷酸钠和氟化物的漂白凝胶对牙釉质物理化学、机械和形态学性能的影响。

Influence of bleaching gels formulated with nano-sized sodium trimetaphosphate and fluoride on the physicochemical, mechanical, and morphological properties of dental enamel.

作者信息

Gruba Amanda Scarpin, Nunes Gabriel Pereira, Marques Mariana Takatu, Danelon Marcelle, Alves Renata de Oliveira, de Toledo Priscila Toninatto Alves, Briso André Luiz Fraga, Delbem Alberto Carlos Botazzo

机构信息

Department of Preventive and Restorative Dentistry, Araçatuba School of Dentistry, Sao Paulo State University (UNESP), Araçatuba, SP, Brazil.

Department of Preventive and Restorative Dentistry, Araçatuba School of Dentistry, Sao Paulo State University (UNESP), Araçatuba, SP, Brazil.

出版信息

J Dent. 2023 Dec;139:104743. doi: 10.1016/j.jdent.2023.104743. Epub 2023 Oct 13.

Abstract

OBJECTIVES

To evaluate in vitro the effects of sodium fluoride (F) and nano-sized sodium trimetaphosphate (TMPnano) added to a 35% hydrogen peroxide (HO) bleaching gel on the color alteration, enamel mechanical and morphological properties, and HO transamelodentinal diffusion.

MATERIALS AND METHODS

Bovine enamel/dentin discs (n = 180) were divided according to the bleaching gel: 35% HO (HP); 35% HO + 0.1% F (HP/F); 35% HO + 1% TMPnano (HP/TMPnano); 35% HO + 0.1% F + 1% TMPnano (HP/F/TMPnano) and 35% HO + 2% calcium gluconate (HP/Ca). The gels were applied 3 times by 40 min; once each 7-day. The Commission Internationale de l'Eclairage (CIE) Lab* total color alteration (ΔE), color alteration by CIEDE2000 (ΔE), whitening index (ΔWI), surface (SH) and cross-sectional hardness (ΔKHN), surface roughness (Ra), and transamelodentinal diffusion were determined. Enamel surfaces were evaluated by Scanning Electron Microscopy (SEM) and X-ray Dispersive Energy (EDX). Data were submitted to ANOVA, followed by the Student-Newman-Keuls test (p <0.05).

RESULTS

ΔE, ΔE, and ΔWID were similar among the gels that promoted a bleaching effect after treatment (p <0.001). Mineral loss (SH and ΔKHN), Ra, and HO diffusion were lower for HP/F/TMPnano; the HP and HP/Ca groups presented the highest values (p <0.001). For SEM/EDX, surface changes were observed in all bleached groups, but less intense with TMPnano.

CONCLUSIONS

Gels containing F/TMPnano do not interfere with the bleaching effect and reduce enamel demineralization, roughness, HO diffusion, and morphological changes.

CLINICAL RELEVANCE

Whitening gels containing F/TMPnano can be used as a new strategy to increase safety and maintain clinical performance.

摘要

目的

在体外评估添加到35%过氧化氢(HO)漂白凝胶中的氟化钠(F)和纳米级三聚磷酸钠(TMPnano)对颜色改变、牙釉质机械性能和形态学性能以及HO经牙本质小管扩散的影响。

材料与方法

根据漂白凝胶将牛牙釉质/牙本质圆盘(n = 180)进行分组:35% HO(HP);35% HO + 0.1% F(HP/F);35% HO + 1% TMPnano(HP/TMPnano);35% HO + 0.1% F + 1% TMPnano(HP/F/TMPnano)和35% HO + 2%葡萄糖酸钙(HP/Ca)。凝胶每隔7天涂抹1次,每次40分钟,共涂抹3次。测定国际照明委员会(CIE)Lab*总颜色变化(ΔE)、CIEDE2000颜色变化(ΔE)、美白指数(ΔWI)、表面硬度(SH)和横截面硬度(ΔKHN)、表面粗糙度(Ra)以及经牙本质小管扩散情况。通过扫描电子显微镜(SEM)和X射线能谱分析(EDX)对牙釉质表面进行评估。数据进行方差分析,随后进行Student-Newman-Keuls检验(p <0.05)。

结果

处理后具有漂白效果的凝胶之间,ΔE、ΔE和ΔWID相似(p <0.001)。HP/F/TMPnano组的矿物质损失(SH和ΔKHN)、Ra以及HO扩散较低;HP组和HP/Ca组的值最高(p <0.001)。对于SEM/EDX,在所有漂白组中均观察到表面变化,但TMPnano组的变化较小。

结论

含F/TMPnano的凝胶不影响漂白效果,且能减少牙釉质脱矿、粗糙度、HO扩散和形态学变化。

临床意义

含F/TMPnano的美白凝胶可作为一种提高安全性并维持临床性能的新策略。

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