Ruiken Jan-Paul, Villwock Jörn, Kraume Matthias
Department of Chemical and Process Engineering, Technische Universität Berlin, Ackerstraße 76, 13355 Berlin, Germany.
Micromachines (Basel). 2023 Oct 10;14(10):1923. doi: 10.3390/mi14101923.
A low-impact acoustic levitation system has been developed to study immobilised single drops in liquid-liquid systems. The ability to observe liquid drops several millimetres in diameter for days enables fundamental research into a wide range of mechanisms. Non-invasive optical measurements with excellent optical accessibility are possible. This experimental work provides the basis for mass transfer studies, emphasizing the precise volume determination, signal noise, reproducibility, and the impact of the acoustic field on the drop and its surrounding environment. The setup can be effectively controlled and proves beneficial for research objectives provided that all liquid phases are entirely degassed, and there are no compressible voids present within the liquids. In addition to the precise, uniform, and reliable measurement conditions, we observed no acoustic streaming in the proximity of the drop and there was no significant vibration of the drop. Qualitative observations using rainbow schlieren deflectometry indicate that the nodal or anti-nodal planes of the standing waves can act as barriers to the dispersion of inhomogeneous dissolved substances in the continuous phase.
一种低冲击声悬浮系统已被开发出来,用于研究液-液系统中固定的单滴。能够观察直径达几毫米的液滴数天,这使得对广泛机制进行基础研究成为可能。利用出色的光学可达性进行非侵入式光学测量也是可行的。这项实验工作为传质研究提供了基础,重点在于精确的体积测定、信号噪声、可重复性以及声场对液滴及其周围环境的影响。只要所有液相都完全脱气,且液体中不存在可压缩的空隙,该装置就能得到有效控制,并证明对研究目标有益。除了精确、均匀和可靠的测量条件外,我们还观察到在液滴附近没有声流,并且液滴没有明显振动。使用彩虹纹影偏折术进行的定性观察表明,驻波的节点或反节点平面可作为连续相中不均匀溶解物质扩散的屏障。