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一次性铅笔石墨电极上阿魏酸的伏安法研究

Voltammetric Investigation of Ferulic Acid at Disposable Pencil Graphite Electrode.

作者信息

David Iulia Gabriela, Popa Dana Elena, Buleandra Mihaela, Codreanu Silvia Nicoleta, Croitoru Lorelei, Iordache Laura Andreea, Noor Hassan

机构信息

Department of Analytical Chemistry and Physical Chemistry, Faculty of Chemistry, University of Bucharest, Panduri Av. 90-92, District 5, 050663 Bucharest, Romania.

Department of Surgery, Faculty of Medicine, "Lucian Blaga" University Sibiu, Lucian Blaga Street 25, 550169 Sibiu, Romania.

出版信息

Micromachines (Basel). 2023 Oct 19;14(10):1951. doi: 10.3390/mi14101951.

DOI:10.3390/mi14101951
PMID:37893389
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC10609049/
Abstract

Ferulic acid (FA), a monohydroxycinnamic acid, is an antioxidant with multiple beneficial effects on human health, presenting also importance in the food and cosmetics industry. Its electrochemical behavior was investigated at the disposable and cost-effective pencil graphite electrode (PGE). Cyclic voltammetry emphasized its pH-dependent, diffusion-controlled oxidation. Using the optimized conditions (HB type PGE, Britton Robinson buffer pH 4.56) differential pulse and square-wave voltammetric techniques were applied for its quantitative determination in the range 4.00 × 10-1.00 × 10 mol/L FA. The developed methods were employed for the rapid and simple assessment of the FA content from a commercially available powder designed for cosmetic use.

摘要

阿魏酸(FA),一种单羟基肉桂酸,是一种对人体健康有多种有益作用的抗氧化剂,在食品和化妆品行业也具有重要意义。在一次性且经济高效的铅笔石墨电极(PGE)上研究了其电化学行为。循环伏安法强调了其pH依赖性、扩散控制的氧化过程。采用优化条件(HB型PGE,pH 4.56的 Britton Robinson缓冲液),应用差分脉冲和方波伏安技术在4.00×10⁻¹.00×10 mol/L FA范围内对其进行定量测定。所开发的方法用于快速、简单地评估一种市售化妆品用粉末中的FA含量。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/7675/10609049/0fe6f83e4e30/micromachines-14-01951-g006.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/7675/10609049/ebfef723b645/micromachines-14-01951-g001.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/7675/10609049/88d73bbc2bd3/micromachines-14-01951-g002.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/7675/10609049/48800be51644/micromachines-14-01951-g003.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/7675/10609049/14a94c210959/micromachines-14-01951-g004.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/7675/10609049/a12f307a8006/micromachines-14-01951-g005.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/7675/10609049/0fe6f83e4e30/micromachines-14-01951-g006.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/7675/10609049/ebfef723b645/micromachines-14-01951-g001.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/7675/10609049/88d73bbc2bd3/micromachines-14-01951-g002.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/7675/10609049/48800be51644/micromachines-14-01951-g003.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/7675/10609049/14a94c210959/micromachines-14-01951-g004.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/7675/10609049/a12f307a8006/micromachines-14-01951-g005.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/7675/10609049/0fe6f83e4e30/micromachines-14-01951-g006.jpg

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Pharmaceutics. 2022 Dec 29;15(1):117. doi: 10.3390/pharmaceutics15010117.
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Antioxidants (Basel). 2022 Nov 22;11(12):2306. doi: 10.3390/antiox11122306.
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Nanomaterials-based electrochemical sensors for the detection of natural antioxidants in food and biological samples: research progress.
基于纳米材料的电化学传感器用于检测食品和生物样品中的天然抗氧化剂:研究进展。
Mikrochim Acta. 2022 Aug 5;189(9):318. doi: 10.1007/s00604-022-05403-5.
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Ferulic acid: An extraordinarily neuroprotective phenolic acid with anti-depressive properties.阿魏酸:一种具有抗抑郁特性的非常神经保护酚酸。
Phytomedicine. 2022 Oct;105:154355. doi: 10.1016/j.phymed.2022.154355. Epub 2022 Jul 22.
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Simultaneous Determination of Caffeic Acid and Ferulic Acid Using a Carbon Nanofiber-Based Screen-Printed Sensor.基于碳纤维纳米纤维的丝网印刷传感器同时测定咖啡酸和阿魏酸。
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