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原子力显微镜观察 3D 打印聚醚醚酮聚合物的表面特性。

Surface characteristics of 3D printed PEEK polymer using atomic force microscopy.

机构信息

School of Mechanical Engineering, Vellore Institute of Technology, Vellore, 632014, India.

School of Mechanical Engineering, Vellore Institute of Technology, Vellore, 632014, India.

出版信息

J Mech Behav Biomed Mater. 2024 Jan;149:106237. doi: 10.1016/j.jmbbm.2023.106237. Epub 2023 Nov 11.

Abstract

High-performance polymer three-dimensional printing is becoming more popular for producing unique parts suitable for different applications. It has been utilized extensively in biomedical applications such as dental prosthetics, surgical equipment, and implants. However, the performance of the material is significantly influenced by its surface qualities, particularly in aspects of its adhesion and biocompatibility. This study involves the fabrication of PEEK specimens S1, S2, S3, and S4 with different printing parameters such as layer height of 0.10 and 0.15 mm and printing speed of 20 and 25 mm/s using a fused deposition modeling process. The surface roughness of the fabricated specimens is measured using atomic force microscopy. The results showed that the printing parameters significantly impact the surface roughness of the PEEK specimens. The surface roughness of specimen S3, printed at a layer height of 0.15 mm and a speed of 20 mm/s, has a low roughness value of 0.017 μm, which is considerable in comparison to the other specimens. In addition to the measurement of surface roughness from roughness profile, the force curve separation graph was plotted and the adhesion force values were calculated for all the specimens to determine the interlayer bonding strength.

摘要

高性能聚合物三维打印技术在生产适合不同应用的独特部件方面越来越受欢迎。它已广泛应用于生物医学领域,如牙科修复体、手术设备和植入物。然而,材料的性能受到其表面质量的显著影响,特别是在其附着力和生物相容性方面。本研究使用熔融沉积建模工艺,制造了具有不同打印参数的 PEEK 标本 S1、S2、S3 和 S4,如层厚为 0.10 和 0.15mm 以及打印速度为 20 和 25mm/s。使用原子力显微镜测量制造标本的表面粗糙度。结果表明,打印参数对 PEEK 标本的表面粗糙度有显著影响。在层厚为 0.15mm 和速度为 20mm/s 的情况下打印的 S3 标本具有较低的粗糙度值 0.017μm,与其他标本相比,这是相当可观的。除了从粗糙度轮廓测量表面粗糙度外,还绘制了力曲线分离图,并计算了所有标本的附着力值,以确定层间结合强度。

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