Park Changbum, Giap Hai-Van, Kwon Jae-Sung, Kim Kyung-Ho, Choi Sung-Hwan, Lee Joon Sang, Lee Kee-Joon
Department of Orthodontics, Institute of Craniofacial Deformity, Yonsei University College of Dentistry, No. 723, 50-1 Yonsei-ro, Seodaemun-gu, Seoul, 03722, Republic of Korea.
Department and Research Institute for Dental Biomaterials and Bioengineering, Yonsei University College of Dentistry, 50-1 Yonsei-ro, Seodaemun-gu, Seoul, 03722, Republic of Korea.
Sci Rep. 2023 Nov 21;13(1):20418. doi: 10.1038/s41598-023-47827-w.
This in vitro study evaluated comprehensively the performances of zirconia brackets with varying yttria proportions in manufacturing advanced orthodontic brackets. Three experimental groups of zirconia brackets were fabricated using yttria-stabilized zirconia (YSZ) materials with different yttria proportions-3 mol% yttria (3Y-YSZ), 4 mol% yttria (4Y-YSZ), and 5 mol% yttria (5Y-YSZ) (Tosoh Ceramic, Japan). A polycrystalline alumina ceramic bracket (3M™ Clarity™ Advanced, MBT 0.022-in. slot) was employed as the control group. Morphological properties, including slot surface structure and dimensions, were examined using scanning electron microscopy and surface profiler analysis. Manufacturing accuracy was assessed with root mean square calculations of trueness and precision. Mechanical properties were tested, encompassing static and kinetic frictional resistance (FR) and fracture strength. Optical stability was evaluated through 20,000 cycles of thermocycling and a 7-day immersion in various coloring agents. Within the limitations of this study, zirconia brackets containing 3 to 5 mol% YSZ presented enhanced reliability in terms of dimensional accuracy and demonstrated favorable optical stability. Notably, owing to its advantageous mechanical properties, the 3Y-YSZ variant showed remarkable potential as an advanced material for fabricating orthodontic brackets.
这项体外研究全面评估了不同氧化钇比例的氧化锆托槽在制造先进正畸托槽方面的性能。使用具有不同氧化钇比例的氧化钇稳定氧化锆(YSZ)材料制备了三组实验性氧化锆托槽——3摩尔%氧化钇(3Y - YSZ)、4摩尔%氧化钇(4Y - YSZ)和5摩尔%氧化钇(5Y - YSZ)(日本东曹陶瓷)。采用多晶氧化铝陶瓷托槽(3M™ Clarity™ Advanced,MBT 0.022英寸槽)作为对照组。使用扫描电子显微镜和表面轮廓仪分析检查包括槽表面结构和尺寸在内的形态学特性。通过真实性和精度的均方根计算评估制造精度。测试了机械性能,包括静摩擦阻力和动摩擦阻力(FR)以及断裂强度。通过20000次热循环和在各种着色剂中浸泡7天来评估光学稳定性。在本研究的局限性内,含有3至5摩尔% YSZ的氧化锆托槽在尺寸精度方面表现出更高的可靠性,并表现出良好的光学稳定性。值得注意的是,由于其有利的机械性能,3Y - YSZ变体作为制造正畸托槽的先进材料显示出显著的潜力。