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饰面技术对氧化锆增强锂硅陶瓷强度的影响。

Finishing technique effect on strength of zirconia-reinforced lithium silicate ceramic.

机构信息

Department of Prosthodontics and Periodontology, University of São Paulo - Bauru School of Dentistry, Sao Paulo, Brazil.

Biomaterials Division, NYU Dentistry, New York, USA.

出版信息

Eur J Oral Sci. 2024 Feb;132(1):e12964. doi: 10.1111/eos.12964. Epub 2023 Dec 7.

Abstract

The aim of this study was to evaluate the effect of two finishing techniques, glazing or polishing, in comparison with the as-cut condition, on the biaxial-flexural-strength (BFS) of a zirconia-reinforced lithium silicate ceramic (ZLS). Cylinders were milled from CAD/CAM blocks and sliced to obtain disc-shaped specimens (ISO6872:2015). Polished and glazed specimens were processed following the manufacturer's instructions. Thirty-three specimens were obtained for each condition and microstructural and BFS/fractographic characterizations were performed. BFS and roughness data were analyzed using Weibull statistics and ANOVA one-way with Tukey post-hoc test, respectively. While a rougher surface was observed for as-cut specimens, smoother surfaces were observed for polished and glazed ZLS at microscopical evaluation and confirmed through surface-roughness evaluation. X-ray spectra depicted a glass phase for all groups and characteristic metasilicate, lithium disilicate, and lithium phosphate peaks for the as-cut and polished specimens. Glazed specimens showed higher characteristic strength than polished and as-cut specimens, which did not differ significantly. While higher Weibull-modulus was observed for the polished than for the as-cut specimens, no statistically significant differences were noted between glazed and polished, and between glazed and as-cut specimens. ZLS presents higher strength when glazed, and polishing increases the structural reliability of the material relative to the as-cut condition. Both finishing techniques reduced surface roughness similarly.

摘要

本研究旨在评估两种后处理技术(上釉或抛光)与初始切割状态相比,对氧化锆增强硅酸锂陶瓷(ZLS)的双轴弯曲强度(BFS)的影响。从 CAD/CAM 块中铣削出圆柱体,并将其切割成圆盘状试件(ISO6872:2015)。按照制造商的说明对抛光和上釉的试件进行处理。每个条件下获得 33 个试件,并进行微观结构和 BFS/断口形貌特征分析。使用威布尔统计和单因素方差分析(ANOVA)与 Tukey 事后检验分别分析 BFS 和粗糙度数据。虽然初始切割试件的表面较粗糙,但抛光和上釉的 ZLS 试件在微观评估和表面粗糙度评估中表现出更光滑的表面。X 射线能谱显示所有组均存在玻璃相,以及初始切割和抛光试件存在特征的偏硅酸锂、二硅酸锂和磷酸锂峰。上釉试件的特征强度高于抛光和初始切割试件,但差异无统计学意义。虽然抛光试件的威布尔模数高于初始切割试件,但抛光和初始切割试件、以及上釉和初始切割试件之间无统计学差异。上釉可提高 ZLS 的强度,抛光相对于初始切割状态提高了材料的结构可靠性。两种后处理技术均能降低表面粗糙度。

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