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基于牛至精油微胶囊/大豆分离蛋白/羧甲基纤维素钠的活性薄膜的制备及特性研究。

Preparation and characterization of active films based on oregano essential oil microcapsules/soybean protein isolate/sodium carboxymethyl cellulose.

机构信息

School of Agricultural Engineering and Food Science, Shandong University of Technology, Zibo 255000, China.

School of Agricultural Engineering and Food Science, Shandong University of Technology, Zibo 255000, China.

出版信息

Int J Biol Macromol. 2024 Feb;258(Pt 2):128985. doi: 10.1016/j.ijbiomac.2023.128985. Epub 2023 Dec 27.

Abstract

This study aimed to prepare oregano essential oil microcapsules (EOMs) by the active coalescence method using gelatin and sodium alginate as wall materials and oregano essential oil (OEO) as the core material. EOMs were added to the soybean protein isolate (SPI)/sodium carboxymethyl cellulose (CMC) matrix to prepare SPI-CMC-EOM active films, and the physical and chemical features of the active films and EOMs were characterized. The results showed that the microencapsulated OEO could protect its active ingredients. Scanning electron microscopy results showed that EOMs were highly compatible with the film matrix. The solubility of active films decreased upon adding EOMs, and their ultraviolet resistance and thermal stability also improved. When the added amount of EOMs was 5 %, the active films had the best mechanical properties and the lowest water vapor permeability. The active films prepared under this condition had excellent comprehensive performance. Also, adding EOMs considerably enhanced the antioxidant of the active films and endowed them with antibacterial properties. The application of the SPI-CMC-EOM films to A. bisporus effectively delayed senescence and maintained the freshness of the postharvest A. bisporus. This study provided a theoretical foundation for the incorporation of EOMs into active films based on biological materials.

摘要

本研究旨在采用活性复凝聚法,以明胶和海藻酸钠为壁材,以牛至精油(OEO)为芯材,制备牛至精油微胶囊(EOMs)。将 EOMs 添加到大豆分离蛋白(SPI)/羧甲基纤维素钠(CMC)基质中,制备 SPI-CMC-EOM 活性薄膜,并对活性薄膜和 EOMs 的物理化学性质进行了表征。结果表明,微胶囊化的 OEO 可以保护其活性成分。扫描电子显微镜结果表明,EOMs 与薄膜基质高度相容。添加 EOMs 后,活性薄膜的溶解度降低,其抗紫外线性和热稳定性也得到提高。当添加量为 5%时,活性薄膜具有最佳的机械性能和最低的水蒸气透过率。在此条件下制备的活性薄膜具有优异的综合性能。此外,添加 EOMs 可显著提高活性薄膜的抗氧化性能,并赋予其抗菌性能。将 SPI-CMC-EOM 薄膜应用于双孢蘑菇,可有效延缓其衰老,保持其采后新鲜度。本研究为将 EOMs 掺入基于生物材料的活性薄膜提供了理论基础。

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