Bahtiti Nawal H, Elgammal Walid E, Ali Ali A, Belal Amany, Abdullah Omeima, Ghoneim Mohammed M, Qenawy Mohmmad S, Abdou Moaz M
Faculty of Arts & Science, Applied Science Private University, Amman 11931, Jordan.
Department of Chemistry, Faculty of Science, Al-Azhar University, Nasr City, Cairo 11751, Egypt.
ACS Omega. 2023 Dec 19;9(1):447-455. doi: 10.1021/acsomega.3c05905. eCollection 2024 Jan 9.
This study synthesizes and characterizes a series of disperse dyes based on azo Schiff bases, compounds -. Their structures were identified using various analytical techniques, such as FT-IR, H/C NMR, and mass spectrometry. The study's primary objective was to investigate the behavior of disperse dyes - when used for dyeing polyester fabrics under different conditions, including variations in time, temperature, shade, and pH. The polyester fabric was chosen for this research due to its wide usage and popularity in the textile industry. By examining the effect of temperature and time on the dyeing process, it was observed that increasing the dyeing temperature from low to high (ranging from 90 to 120 °C) and extending the dyeing time from 10 to 30 min resulted in higher / values for the polyester samples dyed with disperse dyes. Additionally, dyes and exhibited the most excellent / values among the tested dyes. Furthermore, the study found that dye showed the best dyeing performance as the pH of the dye bath increased to 6.
本研究合成并表征了一系列基于偶氮席夫碱的分散染料,即化合物-。使用各种分析技术,如傅里叶变换红外光谱(FT-IR)、氢/碳核磁共振(H/C NMR)和质谱法来鉴定它们的结构。该研究的主要目的是研究分散染料-在不同条件下用于聚酯织物染色时的行为,这些条件包括时间、温度、色泽和pH值的变化。由于聚酯织物在纺织工业中的广泛使用和普及,因此选择其用于本研究。通过研究温度和时间对染色过程的影响,观察到将染色温度从低到高(范围为90至120°C)升高以及将染色时间从10分钟延长至30分钟,会使用分散染料染色的聚酯样品的/值更高。此外,在测试的染料中,染料 和 表现出最优异的/值。此外,研究发现随着染浴pH值增加到6,染料 表现出最佳的染色性能。