6-羟基-1,2-二氢吡啶-2-酮的合成与晶体学表征
Synthesis and crystallographic characterization of 6-hydroxy-1,2-dihydropyridin-2-one.
作者信息
Phillips Sara K, Brancato Savannah G, MacMillan Samantha N, Snider Mark J, Roering Andrew J, Hicks Katherine A
机构信息
Department of Chemistry, The State University of New York at Cortland, Cortland, New York 13045, USA.
Department of Chemistry and Chemical Biology, Cornell University, Ithaca, New York 14853, USA.
出版信息
Acta Crystallogr E Crystallogr Commun. 2023 Nov 14;79(Pt 12):1147-1150. doi: 10.1107/S205698902300974X. eCollection 2023 Dec 1.
The title compound, CHNO, is a hy-droxy-lated pyridine ring that has been studied for its involvement in microbial degradation of nicotinic acid. Here we describe its synthesis as a formic acid salt, rather than the standard hydro-chloride salt that is commercially available, and its spectroscopic and crystallographic characterization.
标题化合物CHNO是一个羟基化的吡啶环，因其参与烟酸的微生物降解而受到研究。在此，我们描述了它作为甲酸盐而非市售标准盐酸盐的合成方法，以及它的光谱和晶体学表征。
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