Post-Graduate Program in Oral Sciences, Center for Development of Advanced Materials, Division of Prosthodontics-Biomaterials, Federal University of Santa Maria (UFSM), Santa Maria, Brazil.
Department of Dental Materials Science, Academic Centre for Dentistry Amsterdam (ACTA), Universiteit Van Amsterdam and Vrije Universiteit, Amsterdam, North Holland, the Netherlands.
Clin Oral Investig. 2024 Feb 14;28(2):149. doi: 10.1007/s00784-024-05542-4.
The study aims to evaluate the shear bond and flexural strength fatigue behavior of yttrium-stabilized zirconia (4YSZ) repaired using different resin composites.
Cylindric specimens of 4YSZ were obtained for the bond strength (Ø = 6 mm, 1.5 mm of thickness) and biaxial flexural strength (Ø = 15 mm, 1 mm of thickness) fatigue tests and divided into 3 groups according to the repair resin composite: EVO (nanohybrid), BULK (bulk-fill), and FLOW (flowable). The zirconia surface was air-abraded with alumina particles, a 10-methacryloyloxydecyl dihydrogen phosphate (10-MDP) primer was applied, and the resin composite was build-up over the zirconia. Fatigue shear bond strength and flexural fatigue strength tests were performed (n = 15). One-way ANOVA and Tukey post hoc tests were carried out for both outcomes, besides scanning electron microscopy and finite element analysis.
The repair material affected the fatigue shear bond strength of zirconia ceramic. The BULK group (18.9 MPa) depicted higher bond strength values than FLOW (14.8 MPa) (p = 0.04), while EVO (18.0 MPa) showed similar results to both groups. No effect was observed for the mechanical behavior (p = 0.53). The stress distribution was similar for all groups.
The repair of yttrium-stabilized zirconia (4YSZ) ceramics with bulk-fill resin composites was the best option for high fatigue bond strength. However, the fatigue mechanical performance was similar regardless of the applied repair material.
The repair of yttrium-stabilized zirconia (4YSZ) monolithic restorations may be performed with nanohybrid and bulk-fill resin composites in order to promote longevity in the treatment.
本研究旨在评估不同树脂复合材料修复氧化钇稳定氧化锆(4YSZ)的剪切粘结强度和弯曲强度疲劳性能。
为了进行粘结强度(Ø=6mm,厚度为 1.5mm)和双轴弯曲强度疲劳测试,获得了 4YSZ 的圆柱形试件,并根据修复用树脂复合材料将试件分为 3 组:EVO(纳米混合)、BULK(块状填充)和 FLOW(流动)。用氧化铝颗粒对氧化锆表面进行气喷砂处理,涂覆 10-甲氧基癸基二氢磷酸酯(10-MDP)底漆,并在氧化锆上堆积树脂复合材料。进行了疲劳剪切粘结强度和弯曲疲劳强度测试(n=15)。对两种结果都进行了单因素方差分析和 Tukey 事后检验,此外还进行了扫描电子显微镜和有限元分析。
修复材料影响氧化锆陶瓷的疲劳剪切粘结强度。BULK 组(18.9MPa)的粘结强度值高于 FLOW 组(14.8MPa)(p=0.04),而 EVO 组(18.0MPa)与两组的结果相似。机械性能没有影响(p=0.53)。所有组的应力分布都相似。
对于高疲劳粘结强度,氧化钇稳定氧化锆(4YSZ)陶瓷的修复使用块状填充树脂复合材料是最佳选择。然而,无论应用何种修复材料,疲劳力学性能都相似。
为了提高治疗的耐久性,氧化钇稳定氧化锆(4YSZ)整体修复体的修复可以使用纳米混合和块状填充树脂复合材料。