Post-Graduate Program in Oral Science, Prosthodontics Unit, Faculty of Dentistry, Federal University of Santa Maria (UFSM), Santa Maria, Rio Grande do Sul State, Brazil.
Department of Dental Materials Science, Academic Centre for Dentistry Amsterdam (ACTA), Universiteit van Amsterdam and Vrije Universiteit, Amsterdam, North Holland, The Netherlands.
Dent Mater. 2022 Dec;38(12):1910-1920. doi: 10.1016/j.dental.2022.09.008. Epub 2022 Oct 10.
To explore the effect of resin cement viscosities on the shear bond strength under static and fatigue load of lithium disilicate and dentin substrates.
Bonded tri-layer samples (lithium disilicate ceramic cylinder, resin cement, and substrate - ceramic or dentin) was performed considering 2 factors (n = 15): "resin cement viscosity" (high, HV; or low, LV) and "loading mode" (static, s-SBS; or fatigue shear bond strength, f-SBS). The specimens were subjected to s-SBS (1 mm/min, 1 kN load cell) and f-SBS (cyclic fatigue, initial load: 10 N; step-size: 5 N; 10,000 cycles/step; underwater). Failure mode, topography, and finite element analysis (FEA) were performed.
The resin cement viscosity did not influence the s-SBS and f-SBS of lithium disilicate substrate; however, it affected the bond strength to dentin, with HV presenting the worst fatigue behavior (f-SBS = 6.89 MPa). Cyclic loading in shear testing induced a notorious detrimental effect with a relevant decrease (16-56 %) in bond strength and survival rates, except for dentin substrate and LV. Most failures were adhesive. A distinct pattern comparing the disilicate and dentin was identified and FEA demonstrated that there was a stress concentration on the top of the cement layer.
Cyclic fatigue loading in shear testing has detrimental effects on the adhesive behavior and survival probabilities of bonded lithium disilicate sets, regardless of resin cement viscosity. In contrast, resin cement viscosity affects the bond strength and the survival rates of dentin substrate submitted to cyclic loading mode, in which a low viscosity results in better performance.
研究在静态和疲劳负荷下,树脂水泥的粘度对锂硅二酸盐和牙本质基底的剪切结合强度的影响。
考虑了 2 个因素(n=15)进行了三层粘结样品(锂硅二酸盐陶瓷圆柱体、树脂水泥和基底-陶瓷或牙本质):“树脂水泥粘度”(高 HV;或低 LV)和“加载模式”(静态 s-SBS;或疲劳剪切结合强度 f-SBS)。将试件进行 s-SBS(1mm/min,1kN 传感器)和 f-SBS(循环疲劳,初始负载:10N;步长:5N;10000 次/步;水下)测试。对失效模式、形貌和有限元分析(FEA)进行了分析。
树脂水泥的粘度并不影响锂硅二酸盐基底的 s-SBS 和 f-SBS,但会影响对牙本质的粘结强度,其中 HV 表现出最差的疲劳行为(f-SBS=6.89MPa)。在剪切试验中循环加载会产生明显的不利影响,粘结强度和存活率显著下降(16%-56%),牙本质基底和 LV 除外。大多数失效是粘结性的。确定了一种明显的区分硅二酸盐和牙本质的模式,FEA 表明在水泥层顶部存在应力集中。
在剪切试验中循环疲劳加载对粘结性行为和粘结的锂硅二酸盐的存活率有不利影响,与树脂水泥的粘度无关。相比之下,树脂水泥的粘度会影响牙本质基底在循环加载模式下的粘结强度和存活率,其中低粘度的性能更好。