Kirmali Omer, Kapdan Alper, Harorli Osman Tolga, Barutcugil Cagatay, Ozarslan Mehmet Mustafa
Department of Prosthodontics, Faculty of Dentistry, Akdeniz University , Antalya , Turkey.
Acta Odontol Scand. 2015 Jan;73(1):28-32. doi: 10.3109/00016357.2014.946963. Epub 2014 Nov 6.
The aim of this study was to evaluate the shear bond strength of composite resin in five different repair systems.
Sixty specimens (7 mm in diameter and 3 mm in height) of zirconia ceramic were fabricated. All specimen surfaces were prepared with a 30 µm fine diamond rotary cutting instrument with water irrigation for 10 s and dried with oil-free air. Specimens were then randomly divided into six groups for the following different intra-oral repair systems (n = 10): Group 1, control group; Group 2, Cojet system (3M ESPE, Seefeld, Germany); Group 3, Cimara® System (Voco, Cuxhaven, Germany); Group 4, Z-Prime Plus System (Bisco Inc., Schaumburg, IL); Group 5, Clearfil™ System (Kuraray, Osaka, Japan); and Group 6, Z-Bond System (Danville, CA). After surface conditioning, a composite resin Grandio (Voco, Cuxhaven, Germany) was applied to the zirconia surface using a cylindrical mold (5 mm in diameter and 3 mm in length) and incrementally filled up, according to the manufacturer's instructions of each intra-oral system. Each specimen was subjected to a shear load at a crosshead speed of 1 mm/min until fracture. One-way analysis of variance (ANOVA) and Tukey post-hoc tests were used to analyze the bond strength values.
There were significant differences between Groups 2-6 and Group 1. The highest bond strength values were obtained with Group 2 (17.26 ± 3.22) and Group 3 (17.31 ± 3.62), while the lowest values were observed with Group 1 (8.96 ± 1.62) and Group 6 (12.85 ± 3.95).
All repair systems tested increased the bond strength values between zirconia and composite resin that used surface grinding with a diamond bur.
本研究旨在评估五种不同修复系统中复合树脂的剪切粘结强度。
制作60个氧化锆陶瓷试件(直径7mm,高3mm)。所有试件表面均使用带水冷却的30μm精细金刚石旋转切割器械处理10秒,并用无油空气吹干。然后将试件随机分为六组,用于以下不同的口腔内修复系统(n = 10):第1组,对照组;第2组,Cojet系统(德国3M ESPE公司,塞费尔德);第3组,Cimara®系统(德国Voco公司,库克斯港);第4组,Z-Prime Plus系统(美国伊利诺伊州绍姆堡市Bisco公司);第5组,Clearfil™系统(日本大阪可乐丽公司);第6组,Z-Bond系统(美国加利福尼亚州丹维尔市)。表面处理后,按照各口腔内系统制造商的说明,使用圆柱形模具(直径5mm,长3mm)将复合树脂Grandio(德国Voco公司,库克斯港)涂覆在氧化锆表面,并逐层填充。每个试件以1mm/min的十字头速度承受剪切载荷直至断裂。采用单因素方差分析(ANOVA)和Tukey事后检验分析粘结强度值。
第2 - 6组与第1组之间存在显著差异。第2组(17.26 ± 3.22)和第3组(17.31 ± 3.62)获得的粘结强度值最高,而第1组(8.96 ± 1.62)和第6组(12.85 ± 3.95)的值最低。
所有测试的修复系统均提高了使用金刚石车针进行表面磨削的氧化锆与复合树脂之间的粘结强度值。