Deisenroth David C, Mekhontsev Sergey, Lane Brandon, Hanssen Leonard, Zhirnov Ivan, Khromchenko Vladimir, Grantham Steven, Cardenas-Garcia Daniel, Donmez Alkan
National Institute of Standards and Technology, Gaithersburg, MD 20899, USA.
Karlstad University, 651 88 Karlstad, Sweden.
J Res Natl Inst Stand Technol. 2021 Aug 10;126:126013. doi: 10.6028/jres.126.013. eCollection 2021.
This paper describes advances in measuring the characteristic spatial distribution of surface temperature and emissivity during laser-metal interaction under conditions relevant for laser powder bed fusion (LPBF) additive manufacturing processes. Detailed descriptions of the measurement process, results, and approaches to determining uncertainties are provided. Measurement uncertainties have complex dependencies on multiple process parameters, so the methodology is demonstrated on one set of process parameters and one material. Well-established literature values for high-purity nickel solidification temperature and emissivity at the solidification temperature were used to evaluate the predicted uncertainty of the measurements. The standard temperature measurement uncertainty is found to be approximately 0.9% of the absolute temperature (16 AC), and the standard relative emissivity measurement uncertainty is found to be approximately 8% at the solidification point of high-purity nickel, both of which are satisfactory. This paper also outlines several potential sources of test uncertainties, which may require additional experimental evaluation. The largest of these are the metal vapor and ejecta that are produced as process by-products, which can potentially affect the imaging quality, reflectometry results, and thermal signature of the process, while also affecting the process of laser power delivery. Furthermore, the current paper focuses strictly on the uncertainties of the emissivity and temperature measurement approach and therefore does not detail a variety of uncertainties associated with experimental controls that must be evaluated for future generation of reference data.
本文描述了在与激光粉末床熔融(LPBF)增材制造工艺相关的条件下,测量激光与金属相互作用过程中表面温度和发射率特征空间分布的进展。文中提供了测量过程、结果以及确定不确定性的方法的详细描述。测量不确定性对多个工艺参数具有复杂的依赖性,因此该方法在一组工艺参数和一种材料上进行了演示。利用高纯度镍凝固温度和凝固温度下发射率的既定文献值来评估测量的预测不确定性。发现标准温度测量不确定性约为绝对温度的0.9%(16℃),在高纯度镍的凝固点处,标准相对发射率测量不确定性约为8%,两者均令人满意。本文还概述了测试不确定性的几个潜在来源,可能需要进行额外的实验评估。其中最大的来源是作为工艺副产品产生的金属蒸汽和喷射物,它们可能会影响成像质量、反射测量结果和工艺的热特征,同时也会影响激光功率传输过程。此外,本文严格聚焦于发射率和温度测量方法的不确定性,因此未详细说明与实验控制相关的各种不确定性,而这些不确定性对于未来生成参考数据必须进行评估。