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不同多层氧化锆牙科材料的抗弯强度及形态学研究

Flexural Strength and Morphological Study of Different Multilayer Zirconia Dental Materials.

作者信息

Labetić Andrea, Klaser Teodoro, Skoko Željko, Jakovac Marko, Žic Mark

机构信息

University of Zagreb School of Dental Medicine, Gunduliceva 5, 10000 Zagreb, Croatia.

Ruder Boskovic Institute, P.O. Box 180, 10000 Zagreb, Croatia.

出版信息

Materials (Basel). 2024 Mar 1;17(5):1143. doi: 10.3390/ma17051143.

Abstract

Nowadays, yttria (Y)-stabilized ZrO (Y-TZP) is the most commonly used material in dental prosthetics. Y-TZP dental ceramics are mainly stabilized via the addition of 3 mol% yttrium oxide (YO). These ceramics exhibit excellent mechanical properties, including high flexural strength, fracture toughness, elastic modulus, etc. Some manufacturers have recently introduced a new class of dental materials with multilayer composition with the aim of combining the advantages of adding more or less YO to the ceramic composition in one Y-TZP material. The flexural strength values of multilayer Y-TZP may vary depending on the dimensions of the specimen, layer distributions, and especially the layer exposed on the maximum tension side, i.e., loading configuration. Although previous studies have examined the flexural strength of separate Y-TZP layers, capturing the flexural strength of multilayer Y-TZP is still challenging. However, one should keep in mind that multilayer flexural strength is important for clinical indications. The objective of this study is to compare the flexural strength of three distinct multilayer translucent Y-TZP materials made up of layers with different Y contents. Rectangular samples (2 mm × 2 mm × 16 mm) were prepared from CAD/CAM discs using the milling machine Programill PM7 (Ivoclar Vivadent AG). Milled bars were tested for flexural strength in a three-point bending test (ISO 6872:2015) using a universal testing machine (Inspekt Duo 5kN; Hegewald & Peschke, Nossen, Germany) at a crosshead speed of 0.5 mm/min. Representative samples of each type of material were selected for quantitative and qualitative analysis of the microstructure. Representative samples of each type of material were selected for structural, mechanical, and microstructural analyses.

摘要

如今,氧化钇(Y)稳定的氧化锆(Y-TZP)是牙科修复中最常用的材料。Y-TZP牙科陶瓷主要通过添加3摩尔%的氧化钇(YO)来实现稳定。这些陶瓷具有优异的机械性能,包括高弯曲强度、断裂韧性、弹性模量等。最近,一些制造商推出了一类新型的多层结构牙科材料,目的是在一种Y-TZP材料中结合在陶瓷成分中或多或少添加YO的优点。多层Y-TZP的弯曲强度值可能会因试样尺寸、层分布,尤其是最大拉伸侧暴露的层(即加载配置)而有所不同。尽管先前的研究已经考察了单独的Y-TZP层的弯曲强度,但获取多层Y-TZP的弯曲强度仍然具有挑战性。然而,应该记住,多层弯曲强度对于临床应用很重要。本研究的目的是比较三种由不同Y含量的层组成的不同多层半透明Y-TZP材料的弯曲强度。使用铣床Programill PM7(义获嘉伟瓦登特股份公司)从CAD/CAM圆盘制备矩形样品(2毫米×2毫米×16毫米)。使用万能试验机(Inspekt Duo 5kN;德国诺森的黑格瓦尔德与佩施克公司)以0.5毫米/分钟的十字头速度在三点弯曲试验(ISO 6872:2015)中测试铣削棒的弯曲强度。选择每种材料类型的代表性样品进行微观结构的定量和定性分析。选择每种材料类型的代表性样品进行结构、机械和微观结构分析。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/4edd/10934541/7fa610171dd2/materials-17-01143-sch001.jpg

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