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评估生物活性玻璃改性通用多模式胶粘剂的物理性能及其对人工诱导龋损牙本质的粘结潜力。

Assessment of physical properties of bioactive glass-modified universal multimode adhesive and its bonding potential to artificially induced caries affected dentin.

机构信息

Dental Biomaterials Department, Faculty of Dentistry, Ain Shams University, African Union Organization Street, Abbasia, Cairo, 11566, Egypt.

出版信息

BMC Oral Health. 2024 Apr 5;24(1):423. doi: 10.1186/s12903-024-04175-z.

Abstract

BACKGROUND

To evaluate the physical properties of bioactive glass-modified universal multimode adhesive and its micro-tensile bond strength (µTBS) to artificially induced caries-affected dentin.

METHODS

All bond universal adhesive was used in the study. Specimens were divided into 2 main groups: control unmodified adhesive and 5 wt% BAG modified adhesive. The degree of conversion, pH, bioactivity, and viscosity of the adhesives were tested with n = 5 for each test. Micro-tensile bond strength evaluation was done in etch & rinse (ER) and selective-etch (SE) modes, where 24 human molar teeth were used (n = 3), 12 teeth for immediate bond strength, and the other 12 were tested after 6 months of storage in simulated body fluid (SBF).

RESULTS

No significant difference was found between the control and the 5wt% BAG groups regarding the degree of conversion (61.01 ± 0.43 and 60.44 ± 0.61 respectively) and the viscosity (109.77 ± 22.3 and 124.3 ± 9.92 respectively). The control group revealed significantly lower pH values than the 5wt% BAG group (3.16 ± 0.5 and 4.26 ± 0.09 respectively). Immediate bond strength results revealed that the 5wt% BAG in the ER mode had the highest bond strength followed by the control group in the ER mode (44.16 ± 7.53 and 44.00 ± 7.96 respectively). SE groups showed that the immediate strength of the 5wt% BAG group was higher than the control group (42.09 ± 6.02 and 39.29 ± 6.64 respectively). After 6 months of storage, bond strength results revealed a decrease in bond strength values for the control groups but not for the 5wt% BAG in both application modes.

CONCLUSIONS

The incorporation of BAG (5wt%) improved the universal adhesive micro-tensile bond strength and bond durability for both adhesive application modes without affecting its degree of conversion or viscosity.

摘要

背景

评估生物活性玻璃改性通用多模式胶粘剂的物理性能及其对人工龋损牙本质的微拉伸粘结强度(µTBS)。

方法

本研究使用了所有的通用粘结剂。将标本分为 2 个主要组:对照组(未改性的通用粘结剂)和 5wt% BAG 改性的粘结剂。每组进行 5 次测试,测试粘结剂的转化率、pH 值、生物活性和粘度。微拉伸粘结强度评估分别在蚀刻冲洗(ER)和选择性蚀刻(SE)模式下进行,使用 24 个人类磨牙(n=3),其中 12 个牙齿用于即时粘结强度,其余 12 个在模拟体液(SBF)中储存 6 个月后进行测试。

结果

在转化率(分别为 61.01±0.43 和 60.44±0.61)和粘度(分别为 109.77±22.3 和 124.3±9.92)方面,对照组和 5wt%BAG 组之间没有显著差异。对照组的 pH 值明显低于 5wt%BAG 组(分别为 3.16±0.5 和 4.26±0.09)。即时粘结强度结果显示,ER 模式下的 5wt%BAG 组具有最高的粘结强度,其次是 ER 模式下的对照组(分别为 44.16±7.53 和 44.00±7.96)。SE 组显示,5wt%BAG 组的即时强度高于对照组(分别为 42.09±6.02 和 39.29±6.64)。储存 6 个月后,对照组的粘结强度值下降,但在两种应用模式下,5wt%BAG 组的粘结强度均未下降。

结论

在不影响通用粘结剂转化率或粘度的情况下,加入 BAG(5wt%)可提高通用粘结剂的微拉伸粘结强度和粘结耐久性,适用于两种粘结剂应用模式。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/69e0/10998361/d64be522109c/12903_2024_4175_Fig1_HTML.jpg

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