Felicioni Stefano, Aversa Alberta, Librera Erica, Bondioli Federica, Fino Paolo
Department of Applied Science and Technology, Politecnico di Torino, Torino, Italy.
Consorzio Interuniversitario Nazionale per la Scienza e Tecnologia dei Materiali (INSTM), Firenze, Italy.
Sci Technol Adv Mater. 2024 Apr 26;25(1):2346071. doi: 10.1080/14686996.2024.2346071. eCollection 2024.
This current study investigates the effect of Direct Energy Deposition (DED) process conditions on the properties and microstructure of M300 maraging steel samples. The investigation centers on two key factors: laser power and deposition environment. The microstructure of this tool steel is analyzed by computing the Primary Cellular Arm Spacing. The findings revealed a significant influence of both inert atmosphere and laser power on cooling conditions. These different cooling rates influence the phase content as demonstrated by X-Ray Diffraction and Electron Backscatter Diffraction measurements. It was demonstrated the presence of different content of residual austenite at cell boundaries. These distinct microstructural features caused variations in the hardness values of the printed samples. Furthermore, a direct aging heat treatment was implemented, that was chosen from Differential Scanning Calorimetry measurements results. This heat treatment proves effective in achieving consistent hardness increases and eliminated the differences among samples built in different process conditions. This outcome suggests the possibility of selecting the most economically viable DED parameters for optimal results.
本研究调查了直接能量沉积(DED)工艺条件对M300马氏体时效钢样品性能和微观结构的影响。该研究集中在两个关键因素上:激光功率和沉积环境。通过计算初生胞状晶臂间距来分析这种工具钢的微观结构。研究结果表明,惰性气氛和激光功率对冷却条件均有显著影响。如X射线衍射和电子背散射衍射测量所示,这些不同的冷却速率会影响相含量。结果表明,在胞状晶界处存在不同含量的残余奥氏体。这些不同的微观结构特征导致了打印样品硬度值的变化。此外,根据差示扫描量热法测量结果选择实施了直接时效热处理。这种热处理被证明在实现硬度持续增加以及消除在不同工艺条件下制造的样品之间的差异方面是有效的。这一结果表明,有可能选择最经济可行的DED参数以获得最佳结果。